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ICPMS daily performance check report, May 21, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 21, 2002.

NYC-WTC_000053939–000054155

Folder label: “ICPMS 5/21/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD2 60+5 PPB Sample Date/Time: Tuesday, May 21, 2002 12:25:01 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV STD2 60+5 PPB.228 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 20985.738 0.558 0.433 60.19123 0.43ug/L Li 6 48487.790 0.963 48487.790 ug/L > Se-1 45 380451.353 1.079 380451.353 ug/L Cr 52 485116.254 2.418 1.259 59.43516 1.37 ug/L Cr 53 57678.692 2.098 0.150 59.14856 1.20 ug/L Mn 55 786232.203 0.839 2.064 57.98635 1.12 ug/L Co 59 573710.254 1.420 1.508 58.25921 0.39 ug/L Ni 60 118131.137 1.105 0.310 57.81153 1.17 ug/L Cu 63 262506.244 0.996 0.690 57.93674 0.36 ug/L Cu 65 128224.575 0.530 0.337 57.54537 0.66 ug/L Zn 66 85093.320 1.747 0.981 59.35685 1.49 ug/L Zn 67 15160.450 1.083 0.175 59.08369 0.29 ug/L Zn 68 64002.161 1.121 0.738 60.01698 0.45 ug/L > Ge 72 86084.207 1.015 86084.207 ug/L As 75 116123.248 2.543 1.214 59.55627 1.82 ug/L Se 77 11105.040 1.282 0.112 59.27725 0.42 ug/L Se 82 11497.301 3.346 0.135 59.80722 2.64 ug/L As-1 75 100062.800 1.885 99900.131 55.45927 1.89 ug/L Kr 83 4415.116 1.697 -356.184 ug/L Ag 107 594122.898 0.311 0.487 60.29057 0.89 ug/L Cd 111 148638.775 0.389 0.122 59.06864 0.74 ug/L Cd 114 350546.322 1.105 0.287 59.55966 1.56 ug/L > In 115 1219773.095 1.082 1219773.095 ug/L Sb 121 491489.439 1.950 0.403 59.32771 1.09 ug/L Sb 123 378672.876 1.238 0.310 59.64610 0.79 ug/L Ba 135 142790.741 2.105 0.079 60.58282 1.97 ug/L Ba 137 248093.566 0.619 0.136 60.46551 0.71 ug/L Ho 165 1855469.222 1.662 0.005 ug/L Tb 159 1817534.041 0.690 1817534.041 ug/L Hg 201 6693.197 2.074 0.004 5.01140 1.89 ug/L Hg 202 15056.610 1.035 0.008 4.89391 0.52 ug/L TI 205 1686733.315 1.096 0.928 59.50098. 1.27 ug/L Pb 208 2324340.594 0.290 1.278 60.0269! 0.62 ug/L

Sample ID: CCV STD2 60+5 PPB Report Date/Time: Tuesday, May 21, 2002 12:27:23 Page 1

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NYC-WTC_000054015Source: NYC Law Department, mirrored locally

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