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ICPMS daily performance check report, May 21, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 21, 2002.

NYC-WTC_000053939–000054155

Folder label: “ICPMS 5/21/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10604 Sample Date/Time: Tuesday, May 21, 2002 11:41:26 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0604.216 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.667 17.625 0.000 0.00441 101.15 ug/L Li 6 45775.082 0.718 45775.082 ug/L > Se-1 45 351056.469 0.659 351056.469 ug/L Cr 52 5734.199 1.982 0.001 0.03942 34.91 ug/L Cr 53 779.041 10.609 0.001 0.26449 36.51 ug/L Mn 55 319780.490 0.889 0.908 25.50920 0.46 ug/L Co 59 342.010 7.917 0.001 0.02812 9.78 ug/L Ni 60 688.700 3.293 0.002 0.34779 2.96 ug/L Cu 63 4540.179 0.303 0.012 1.04956 0.93 ug/L Cu 65 2163.612 1.506 0.006 1.01052 0.96 ug/L Zn 66 1368.783 0.805 0.008 0.49542 1.48 ug/L Zn 67 369.678 3.752 0.003 0.95271 5.93 ug/L Zn 68 1425.459 3.513 0.011 0.88755 5.54 ug/L > Ge 72 85592.230 0.218 85592.230 ug/L As 75 12557.563 2.431 0.012 0.57327 32.39 ug/L Se 77 1523.836 1.805 0.001 0.41549 44.36 ug/L Se 82 -145.239 81.890 -0.001 -0.29566 209.07 ug/L As-1 75 870.717 2.549 708.047 0.39307 3.13 ug/L Kr 83 4544.515 2.930 -226.785 ug/L Ag 107 603.026 4.066 0.000 0.01778 10.32 ug/L Cd 111 115.669 41.013 0.000 0.01732 106.61 ug/L Cd 114 287.726 36.415 0.000 0.02339 73.38 ug/L > In 115 1220729.441 1.147 1220729.441 ug/L Sb 121 756.373 9.995 0.001 0.08736 9.26 ug/L Sb 123 554.132 13.042 0.000 0.08213 12.74 ug/L Ba 135 43039.413 1.157 0.023 17.89219 0.36 ug/L Ba 137 75427.741 1.308 0.041 18.01340 0.52 ug/L Ho 165 1900517.360 1.736 0.009 ug/L > Tb 159 1853878.953 1.316 1853876.953 ug/L Hg 201 95.001 8.355 0.000 0.03476 19.41 ug/L Hg 202 218.338 10.538 0.000 0.04374 14.80 ug/L TI 205 968.728 4.455 0.000 0.00054 193.90 ug/L Pb 208 6885.747 2.280 0.003 0.12448 1.77 ug/L

Sample ID: AE10604 Report Date/Time: Tuesday, May 21, 2002 11:43:22 Page 1

NYC-WTC_000053979

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