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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10204 Sample Date/Time: Wednesday, May 15,2002 13:08:24 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0204.088 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.667 40.522 -0.000- -0.00576 156.73 ug/L Li 6 54877.432 2.750 54877.432 ug/L > Se-1 45 458437.611 1.189 458437.611 ug/L Cr 52 14745.100 2.386 0.017 0.78300 6.73 ug/L Cr 53 2305.649 1.091 0.004 1.55622 1.02 ug/L Mn 55 533480.748 1.021 1.160 32.15190 0.59 ug/L Co 59 688.700 5.348 0.001 0.04821 7.76 ug/L Ni 60 1359.449 2.300 0.003 0.53621 3.59 ug/L Cu 63 58911.530 0.929 0.128 10.88305 2.11 ug/L Cu 65 28839.298 1.360 0.062 10.95713 2.48 ug/L Zn 66 6660.840 1.440 0.060 3.57043 0.54 ug/L Zn 67 1337.445 1.421 0.012 4.01855 2.01 ug/L Zn 68 5789.234 1.751 0.052 4.14162 0.76 ug/L > Ge 72 99690.744 1.901 99690.744 ug/L As 75 6047.582 2.844 0.012 0.60776 14.07 ug/L Se 77 855.644 2.938 0.002 0.95373 19.80 ug/L Se 82 134.200 12.090 0.002 0.76150 11.02 ug/L As-1 75 1176.088 5.797 1054.086 0.46391 6.47 ug/L Kr 83 1935.892 2.483 -165.372 ug/L Ag 107 882.052 8.561 0.000 0.03756 16.50 ug/L Cd 111 90.335 14.866 0.000 0.00439 100.69 ug/L Cd 114 193.339 15.423 0.000 0.00593 70.01 ug/L In 115 1375893.337 0.959 1375893.337 ug/L Sb 121 720.369 2.493 0.000 0.07713 2.01 ug/L Sb 123 548.544 4.415 0.000 0.07613 5.34 ug/L Ba 135 66429.862 1.561 0.034 22.28558 1.54 ug/L Ba 137 114878.800 0.917 0.058 21.99829 0.80 ug/L Ho 165 2030442.002 0.489 0.010 ug/L > Tb 159 1976998.288 0.126 1976998.288 ug/L Hg 201 84.335 4.792 0.000 0.01049 26.03 ug/L Hg 202 176.337 3.983 0.000 0.00800 24.94 ug/L TI 205 504.352 1.128 -0.000 -0.00671 2.54 ug/L Pb 208 14589.347 0.569 0.006 0.26807 0.78 ug/L

QC Calculated Values

Sample ID: AE10204 Report Date/Time: Wednesday, May 15, 2002 13:10:20 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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