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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10019 Sample Date/Time: Thursday, May 16, 2002 10:48:40 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE10019.140 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.333 31.109 0.000- 0.00813 104.95 ug/L' Li 6 54899.488 0.728 54899.488 ug/L > Sc-1 45 417164.464 1.962 417164.464 ug/L Cr 52 8154.404 1.025 0.005 0.21836 12.13 ug/L Cr 53 1564.817 0.713 0.002 0.77187 3.12 ug/L Mn 55 242444.043 0.175 0.578 16.25586 2.12 ug/L Co 59 389.012 7.166 0.000 0.01750 12.58 ug/L Ni 60 721.369 4.480 0.002 0.31597 5.58 ug/L Cu 63 6373.965 2.239 0.015 1.29023 3.73 ug/L Cu 65 3150.577 0.165 0.007 1.29778 1.91 ug/L Zn 66 3464.361 1.578 0.028 1.63026 2.09 ug/L Zn 67 743.038 4.466 0.006 2.02181 5.97 ug/L Zn 68 3039.872 1.571 0.025 1.98881 1.91 ug/L > Ge 72 95974.578 0.407 95974.578 ug/L As 75 5469.602 4.017 0.007 0.34052 33.27 ug/L Se 77 742.048 0.957 0.001 0.38943 11.61 ug/L Se 82 -67.431 60.879 -0.001 -0.22153 84.14 ug/L As-1 75 832.046 2.717 634.042 0.30924 3.57 ug/L Kr 83 1964.899 0.964 -64.015 ug/L Ag 107 730.705 24.657 -0.000 -0.00621 254.78 ug/L Cd 111 159.336 9.587 0.000 0.02729 21.81 ug/L Cd 114 358.109 6.217 0.000 0.02937 12.31 ug/L > In 115 1335638.257 1.102 1335638.257 ug/L Sb 121 808.044 12.074 0.001 0.08367 12.00 ug/L Sb 123 618.210 9.693 0.000 0.08284 9.57 ug/L Ba 135 44469.284 1.130 0.023 16.13478 1.82 ug/L Ba 137 77821.202 2.052 0.040 16.18546 2.98 ug/L Ho 165 1964356.654 1.057 -0.009 ug/L > Tb 159 1950667.222 1.291 1950667.222 ug/L Hg 201 79.334 22.701 0.000 0.02409 47.36 ug/L Hg 202 170.670 10.552 0.000 0.02540 21.25 ug/L TI 205 677.032 5.415 -0.000 -0.00124 86.39 ug/L Pb 208 4574.164 3.587 0.001 0.05998 6.31 ug/L

Sample ID: AE10019 Report Date/Time: Thursday, May 16, 2002 10:50:36 Page 1

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