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ICPMS daily performance check report, May 15, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10131 Sample Date/Time: Wednesday, May 15, 2002 10:31:44 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cit\AE10131.068 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean, Cone. Mean Cone. RSD Sample Unit ' Be 9 9.667 5.973 -0.000 -0.00385 45.29 ug/L > Li 6 56356.725 1.251 56356.725 ug/L > Se-1 45 466083.485 3.868 466083.485 ug/L Cr 52 8328.897 0.973 0.002 0.11332 21.01 ug/L Cr 53 1149.418 8.145 0.001 0.56057 13.06 ug/L Mn 55 343941.392 0.721 0.735 20.37388 4.38 ug/L Co 59 377.345 7.469 0.001 0.02132 13.90 ug/L Ni 60 857.382 2.917 0.002 0.32623 5.05 ug/L Cu 63 6215.520 1.009 0.013 1.06751 3.67 ug/L Cu 65 2913.496 0.804 0.006 1.01273 3.25 ug/L Zn 66 2331.656 3.249 0.014 0.81861 4.32 ug/L Zn 67 561.356 2.830 0.003 1.17503 3.59 ug/L Zn 68 2342.659 1.465 0.015 1.19551 1.07 ug/L > Ge 72 111803.434 0.739 111803.434 ug/L As 75 6214.125 1.878 0.007 0.35754 19.48 ug/L Se 77 807.282 4.284 0,000 0.21916 88.63 ug/L Se 82 -23.230 252.033 0.000 0.06685 349.01 ug/L As-1 75 1132.749 2.136 1010.747 0.44483 2.39 ug/L Kr 83 2096.263 1.746 -5.001 ug/L Ag 107 439.682 5.610 -0.000 -0.00606 37.83 ug/L Cd 111 131.002 9.255 0.000 0.01403 28.54 ug/L Cd 114 270.831 8.738 0.000 0.01352 22.38 ug/L In 115 1524763.124 0.799 1524763.124 ug/L Sb 121 514.353 4.336 0.000 0.04790 4.06 ug/L Sb 123 380.528 1.879 0.000 0.04568 2.61 ug/L Ba 135 51820.817 1.549 0.025 16.89156 1.23 ug/L Ba 137 91159.754 1.545 0.045 16.96206 0.96 ug/L Ho 165 2089753.906 0.414 0.011 ug/L > Tb 159 2033914.724 0.782 2033914.724 ug/L Hg 201 85.668 21.598 0.000 0.00979 120.77 ug/L Hg 202 171.670 17.323 0.000 0.00522 154.36 ug/L TI 205 752.372 0.277 0.000 0.00044 26.84 ug/L Pb 208 5237.643 1.205 0.001 0.05856 3.47 ug/L

QC Calculated Values

Sample ID: AE10131 Report Date/Time: Wednesday, May 15, 200210:33:41 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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