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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10241 Sample Date/Time: Thursday, May 16, 2002 12:17:52 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0241.164 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 8.000 33.072 0.000 0.00219 283.88 ug/L Li 6 54240.652 3.248 54240.652 ug/L > Se-1 45 419694.135 2.599 419694.135 ug/L Cr 52 7916.191 1.105 0.004 0.18632 16.73 ug/L Cr 53 1143.083 4.409 0.001 0.36533 13.08 ug/L Mn 55 332834.899 1.595 0.790 22.22763 3.91 ug/L Co 59 365.678 7.217 0.000 0.01513 14.56 ug/L NI 60 696.367 1.912 0.002 0.30275 4.21 ug/L Cu 63 5847.939 0.506 0.014 1.17329 2.25 ug/L Cu 65 2815.464 2.878 0.006 1.14856 4.33 ug/L Zn 66 2811.463 0.885 0.022 1.27635 0.96 ug/L Zn 67 600.693 3.798 0.005 1.58256 3.70 ug/L Zn 68 2583.727 . 4.207 0.021 1.66801 4.55 ug/L > Ge 72 93665.356 1.092 93665.356 ug/L As 75 5263.147 4.755 0.006 0.30202 43.60 ug/L Se 77 710.315 5.976 0.001 0.31343 78.09 ug/L Se 82 -48.508 243.960 -0.000 -0.14093 392.48 ug/L As-1 75 668.698 2.681 470.694 0.22957 3.81 ug/L Kr 83 1897.550 2.341 -131.363 ug/L Ag 107 137.336 4.738 -0.000 -0.05949 1.00 ug/L Cd 111 87.001 13.793 0.000 0.00287 159.34 ug/L Cd 114 195.318 10.478 0.000 0.00590 56.72 ug/L > In 115 1271989.446 0.226 1271989.446 ug/L Sb 121 458.683 2.195 0.000 0.04757 2.25 ug/L Sb 123 356.617 8.046 0.000 0.04769 9.33 ug/L Ba 135 43741.454 2.321 0.023 16.58894 1.87 ug/L Ba 137 76188.038 1.079 0.041 16.56379 1.90 ug/L Ho 165 1903345.603 1.760 0.004 ug/L > Tb 159 1866013.471 1.321 1866013.471 ug/L Hg 201 40.334 16.132 -0.000 -0.00051 906.25 ug/L Hg 202 78.001 9.245 -0.000 -0.00060 353.41 ug/L T1 205 523.020 5.604 -0.000 -0.00535 19.22 ug/L Pb 208 3658.327 3.012 0.001 0.04248 4.94 ug/L

Sample ID: AE10241 Report Date/Time: Thursday, May 16,2002 12:19:48 Page 1

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