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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV CAL BK Sample Date/Time: Thursday, May 16, 2002 09:37:23 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cit\ICV CAL BK.129 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 8.000 33.072 0.000 ' 0.00102 615.23 ug/L Li 6 57616.944 1.556 57616.944 ug/L > Sc-1 45 462653.252 5.005 462653.252 ug/L Cr 52 6662.174 2.419 -0.000 -0.02341 77.89 ug/L Cr 53 579.024 1.133 -0.001 -0.21647 12.69 ug/L Mn 55 1658.168 6.969 -0.000 -0.00142 464.62 ug/L Co 59 233.672 4.308 0.000 0.00091 200.19 ug/L Ni 60 34.000 15.563 0.000 0.00149 108.09 ug/L Cu 63 234.005 9.661 0.000 0.00663 89.36 ug/L Cu 65 135.002 10.962 0.000 0.01125 72.23 ug/L Zn 66 706.035 4.881 -0.001 -0.07374 21.63 ug/L Zn 67 150.003 7.211 -0.000 -0.05514 74.21 ug/L Zn 68 565.357 4.202 -0.001 -0.06551 18.98 ug/L > Ge 72 103465.891 1.393 103465.891 ug/L As 75 5183.540 3.462 0.000 0.00781 1031.01 ug/L Se 77 720.704 4.471 -0.000 100594 2610.56 ug/L Se 82 20.742 238.155 0.000 1.17285 119.70 ug/L As-1 75 134.002 7.197 -64.002 1.03122 15.07 ug/L Kr 83 1947.228 1.888 -81.685 ug/L Ag 107 518.020 8.355 -0.000 12815 12.33 ug/L Cd 111 94.335 7.058 0.000 0. 205 129.79 ug/L Cd 114 204.522 9.643 0.000 0.03401 59.98 ug/L > In 115 1415469.820 1.697 1415469.820 ug/L Sb 121 256.006 3.767 0.000 0.02097 2.96 ug/L Sb 123 200.235 7.938 0.000 0.02090 10.55 ug/L Ba 135 38.000 26.316 -0.000 -0.00064 538.06 ug/L Ba 137 58.334 1.979 -0.000 -0.0 3072 42.18 ug/L Ho 165 2050447.487 1.151 0.014 ug/L > Tb 159 1991197.069 0.859 1991197.069 ug/L Hg 201 71.668 5.809 0.000 0.01809 12.91 ug/L Hg 202 159.670 17.718 0.000 0.02120 36.76 ug/L 71 205 735.037 5.760 0.000 0.00013 1129.47 ug/L Pb 208 1997.440 2.186 -0.000 -0.00106 89.59 ug/L

Sample ID: ICV CAL BK Report Date/Time: Thursday, May 16, 2002 09:40:18 Page 1

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