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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV CAL BK Sample Date/Time: Wednesday, May 15, 2002 09:54:36 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cit\ICV CAL BK.061 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean _ Cone. Mean Cone. RSD Sample Unit Be 9 6.333 59.778 -0.000 -0.01498 58.36 ug/L Li 6 61757.062 2.025 61757.062 ug/L Se-1 45 523072.414 1.430 523072.414 ug/L Cr 52 7839.124 1.235 -0.002 0.09321 6.24 ug/L Cr 53 514.687 11.238 0.000 0.02220 170.16 ug/L Mn 55 2287.644 4.682 0.002 0.05217 13.65 ug/L Co 59 127.002 10.236 -0.000 ■0.00091 118.71 ug/L Ni 60 53.334 13.821 0.000 0.00259 111.06 ug/L Cu 63 325.009 3.549 0.000 3.00373 70.00 ug/L Cu 65 173.670 10.778 -0.000 -).00186 336.59 ug/L Zn 66 908.388 7.950 0.001 0.06506 63.30 ug/L Zn 67 181.670 8.744 0.000 0.10274 49.70 ug/L Zn 68 708.702 12.570 0.000 0.03925 166.15 ug/L Ge 72 116959.776 0.961 116959.776 ug/L As 75 5430.645 3.038 -0.001 -).06909 122.73 ug/L Se 77 771.627 1.376 -0.000 -3.09706 85.51 ug/L Se 82 -4.200 1170.206 -0.000 0.02310 810.93 ug/L As-1 75 127.336 15.595 2.000 0.00088 992.89 ug/L Kr 83 2093.262 1.510 -108.360 ug/L Ag 107 2389.351 25.087 -0.008 -0.99930 4.64 ug/L Cd 111 90.335 8.382 0.000 0.01595 14.27 ug/L Cd 114 226.804 7.485 0.000 0.0 2133 9.01 ug/L > In 115 1589916.328 0.926 1589916.328 ug/L Sb 121 63.001 12.397 -0.000 -0.00537 14.60 ug/L Sb 123 50.438 17.664 -0.000 -0.00417 26.12 ug/L Ba 135 84.668 11.349 -0.000 -0.00176 166.88 ug/L Ba 137 141.003 4.965 0.000 0.00085 119.43 ug/L Ho 165 2117552.649 0.377 0.001 ug/L Tb 159 2084715.452 1.346 2084715.452 ug/L Hg 201 97.335 21.971 0.000 0.02381 52.85 ug/L Hg 202 189.671 20.327 0.000 0.01871 55.04 ug/L TI 205 876.051 3.597 0.000 0.01060 12.23 ug/L Pb 208 2647.179 3.773 -0.000 -0.00918 15.08 ug/L

QC Calculated Values

Sample ID: ICV CAL BK Report Date/Time: Wednesday, May 15, 2002 09:57:26 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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