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ICPMS daily performance check report, May 15, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10131 Sample Date/Time: Wednesday, May 15, 2002 10:39:21 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE10131.069 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 18774.555 0.797 0.349. 49.57478 1.36 ug/L Li 6 53698.377 2.147 53698.377 ug/L Sc-1 45 449481.503 1.560 449481.503 ug/L Cr 52 455283.416 4.166 0.997 46.73972 3.35 ug/L Cr 53 55042.011 0.449 0.121 47.17881 1.28 ug/L Mn 55 1099150.948 2.048 2.442 67.67594 1.60 ug/L Co 59 554687.135 2.688 1.234 47.92602 1.27 ug/L Ni 60 118014.933 0.630 0.262 48.99929 1.17 ug/L Cu 63 261620.771 1.331 0.581 49.53656 1.40 ug/L Cu 65 127495.106 0.829 0.283 49.70647 2.29 ug/L Zn 66 93114.368 0.419 0.867 51.92864 1.78 ug/L Zn 67 16058.333 1.493 0.149 50.54546 1.91 ug/L Zn 68 69243.401 0.610 0.644 51.14701 1.57 ug/L > Ge 72 106491.636 1.915 106491.636 ug/L As 75 113376.566 1.870 1.017 50.03831 2.87 ug/L Se 77 11455.835 0.637 0.101 54.28161 2.40 ug/L Se 82 12735.084 2.487 0.120 53.64722 4.34 ug/L As-1 75 103650.689 1.741 103528.687 45.56324 1.74 ug/L Kr 83 2054.253 0.687 -47.011 ug/L Ag 107 527019.062 0.261 0.361 44.63274 2.20 ug/L Cd 111 145603.451 1.816 0.100 47.19702 1.66 ug/L Cd 114 339017.752 1.248 0.232 47.37193 1.88 ug/L > In 115 1460703.766 2.053 1460703.766 ug/L Sb 121 476128.155 1.122 0.326 51.15242 1.01 ug/L Sb 123 366166.803 0.681 0.251 51.17471 1.39 ug/L ' Ba 135 181856.377 1.624 0.091 60.20804 1.53 ug/L Ba 137 317110.331 0.895 0.158 59.92639 1.51 ug/L Ho 165 2054923.144 1.126 0.008 ug/L > Tb 159 2004847.309 1.072 2004847.309 ug/L Hg 201 5829.594 0.584 0.003 3.74170 0.62 ug/L Hg 202 13237.430 0.207 0.007 3.74678 0.89 ug/L TI 205 1682990.296 0.701 0.839 52.27560 1.35 ug/L Pb 208 1998744.637 1.112 0.996 43.42445 0.51 ug/L

QC Calculated Values

Sample ID: AE10131 Report Date/Time: Wednesday, May 15, 2002 10:42:07 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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