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ICPMS daily performance check report, May 14, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD1 30+ 2PPB Sample Date/Time: Tuesday, May 14, 2002 12:05:29 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\rd1\elandata\Datasef\new york city\CCV STD1 30+ 2PPB.040 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean _ Cone. Mean Cone. RSD Sample Unit Be 9 14697.355 2.274 0.025 30.86120 2.11 ug/L > Se-1 45 579472.111 2.232 579472.111 ug/L Cr 52 380887.665 2.385 0.642 30.04762 1.98 ug/L Cr 53 45668.238 1.977 0.077 30.49329 1.30 ug/L Mn 55 631049.121 1.159 1.087 30.29324 1.12 ug/L Ni 60 91305.477 0.535 0.158 29.73766 1.78 ug/L Cu 63 199746.892 1.520 0.344 30.45020 0.71 ug/L Cu 65 96171.311 0.459 0.166 30.63425 1.86 ug/L Zn 66 63979.326 0.834 0.513 30.21231 2.65 ug/L Zn 67 11238.388 0.832 0.090 30.18273 1.05 ug/L Zn 68 47482.181 1.917 0.380 30.04023 0.78 ug/L Ge 72 122941.455 1.824 122941.455 ug/L As 75 81305.754 0.452 0.617 30.08330 1.47 ug/L Se 77 8058.367 0.979 0.059 31.01301 1.92 ug/L Se 82 8483.229 0.522 0.069 30.54429 2.03 ug/L Kr 83 2297.313 0.632 -207.391 ug/L Ag 107 408319.972 1.209 0.251 29.18092 0.68 ug/L > In 115 1627520.007 0.650 1627520.007 ug/L Sb 121 313611.892 0.659 0.193 31.17501 0.22 ug/L Sb 123 240832.911 1.406 0.148 31.48791 0.93 ug/L Ba 135 94876.189 1.434 0.037 28.49710 1.12 ug/L Ba 137 165939.762 0.121 0.064 28.34099 0.64 ug/L Tb 159 2587309.089 0.755 2587309.089 ug/L Hg 201 3298.965 1.883 0.001 2.02060 1.45 ug/L Hg 202 7277.985 1.612 0.003 1.95335 1.42 ug/L Tl 205 1170580.472 0.210 0.452 30.06199 0.55 ug/L Pb 208 1414048.380 0.447 0.545 29.23546 0.55 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 Se-1 45 82.229 Cr 52 Cr 53 Mn 55

Sample ID: CCV STD1 30+ 2PPB Report Date/Time: Tuesday, May 14, 2002 12:07:35 Page 1

NYC-WTC_000053468

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