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ICPMS daily performance check report, April 25, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on April 25, 2002.

NYC-WTC_000053337–000053387

Folder label: “ICPMS 4/25/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD1 30 PPB Sample Date/Time: Thursday, April 25, 2002 15:33:51 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\rd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\dataset\new york city\CCV STD1 30 PPB.712 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 11415.949 3.302 0.024 31.92148 1.93 ug/L Se-1 45 476052.268 1.575 476052.268 ug/L Cr 52 270405.970 2.285 0.553 29.96331 1.49 ug/L Cr 53 31765.065 2.043 0.066 29.92986 0.59 ug/L Mn 55 418695.969 1.999 0.876 30.42958 1.51 ug/L Ni 60 64294.239 1.704 0.135 29.43960 1.41 ug/L Cu 63 149036.719 1.517 0.312 30.08363 1.24 ug/L Cu 65 73797.418 1.175 0.155 30.09411 1.43 ug/L Zn 66 49206.318 1.415 0.525 31.20911 2.52 ug/L Zn 67 8696.246 2.270 0.093 30.15854 2.02 ug/L Zn 68 36401.769 1.024 0.388 30.74832 1.07 ug/L Ge 72 91973.279 2.002 91973.279 ug/L As 75 54875.033 1.309 0.595 29.58736 0.89 ug/L Se 77 5187.772 2.016 0.055 30.68542 4.05 ug/L Se 82 6214.519 0.623 0.066 29.91429 2.54 ug/L Ag 107 296111.791 0.998 0.237 29.26075 1.88 ug/L > In 115 1248227.476 1.454 1248227.476 ug/L Sb 121 249630.566 0.892 0.200 29.67236 0.86 ug/L Sb 123 191812.792 0.481 0.154 29.37379 0.97 ug/L Ba 135 75784.000 0.783 0.045 29.83515 1.72 ug/L Ba 137 131973.421 1.128 0.078 29.75616 0.96 ug/L Ho 165 1679561.204 0.691 0.007 ug/L > Tb 159 1687368.299 1.061 1687368.299 ug/L Hg 201 2223.294 2.476 0.001 2.06536 I 2.05 ug/L Hg 202 4943.060 2.162 0.003 2.02779 1.32 ug/L TI 205 690959.003 1.669 0.409 30.86033 0.66 ug/L Pb 208 940137.345 0.731 0.556 31.15209 0.96 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 113.523 Cr 52 Cr 53 Mn 55

Sample ID: CCV STD1 30 PPB Report Date/Time: Thursday, April 25, 2002 15:36:05 Page 1

NYC-WTC_000053384

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