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ICPMS daily performance check report, April 15, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040648–000040698

Folder label: “ICPMS 4/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD1 30 PPB Sample Date/Time: Monday, April 15, 2002 11:44:30 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\CCV STD1 30 PPB.511 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 13531.872 3.025 1.574 0.025 30.69267 4.51 ug/L Se-1 45 550977.466 550977.466 ug/L Cr 52 306094.886 3.508 0.556 29.34368 3.93 ug/L Cr 53 36943.309 2.379 0.067 ug/L Mn 55 489819.902 2.901 0.889 29.01431 2.45 ug/L NI 60 72509.413 0.454 0.132 27.46298 1.96 ug/L Cu 63 176547.230 2.469 0.320 29.14485 2.46 ug/L Cu 65 85700.398 2.424 0.156 28.66545 2.56 ug/L Zn 66 60455.336 1.940 0.580 31.79098 2.51 ug/L Zn 67 10346.665 5.074 0.099 31.04430 4.58 ug/L Zn 68 41605.758 1.783 0.399 ug/L > Ge 72 104210.944 0.649 104210.944 ug/L As 75 61787.503 1.565 0.593 29.19275 2.12 ug/L Se 77 8353.021 9.654 0.080 46.70967 10.26 ug/L Se 82 7253.299 2.359 0.070 796 r 2.86 ug/L Ag 107 342915.717 0.741 0.237 29.50626 3.14 ug/L Cd 111 87599.090 2.512 0.061 29.57142 1.99 ug/L Cd 114 206686.129 1.483 0.143 29.21043 4.94 ug/L > In 115 1446196.070 3.466 1446196.070 ug/L Sb 121 298221.972 0.678 0.206 30.05940 2.81 ug/L Sb 123 221357.471 0.950 0.153 29.07260 2.55 ug/L Ba 135 89553.316 4.145 0.045 28.14156 3.61 ug/L Ba 137 155186.914 0.498 0.079 27.83010 1.59 ug/L > Tb 159 1968782.124 1.390 1968782.124 ug/L Ho 165 1890802.803 1.547 0.960 ug/L TI 205 812717.386 0.362 0.413 28.29106 1.04 ug/L Pb 208 1113557.470 2.239 0.566 28.92018 1.63 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Se-1 45 Cr 52 Cr 53 Mn 55

Sample ID: CCV STD1 30 PPB Report Date/Time: Monday, April 15, 2002 11:47:10 Page 1

NYC-WTC_000040695

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