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ICPMS daily performance check report, April 16, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040755–000040869

Folder label: “ICPMS 4/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD1 30 PPB Sample Date/Time: Tuesday, April 16,2002 11:22:53 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\CCV STD1 30 PPB.569 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit ' Be 9 13006.765 2.333 0.026 31.67266 4.94 ug/L > Se-1 45 493966.928 2.595 493966.928 ug/L Cr 52 279587.234 1.037 0.549 28.56826 1.93 ug/L Cr 53 35451.683 1.043 0.070 30.97929 2.00 ug/L Mn 55 443201.666 1.682 0.895 29.16531 1.01 ug/L Ni 60 67861.099 2.230 0.137 28.19535 4.80 ug/L Cu 63 157014.019 3.589 0.317 30.01902 1.17 ug/L Cu 65 77896.088 0.548 0.157 28.44143 3.08 ug/L Zn 66 55475.990 1.255 0.579 32.03661 1.84 ug/L Zn 67 9103.648 1.641 0.094 28.89278 1.48 ug/L Zn 68 39721.725 3.531 0.415 31.18523 6.34 ug/L Ge 72 94962.283 2.865 94962.283 ug/L As 75 59511.308 1.294 0.627 29.89042 3.19 ug/L Se 77 5962.363 2.176 0.062 32.75448 0.71 ug/L Se 82 6743.568 1.854 0.070 30.79825 4.60 ug/L Ag 107 317545.095 2.714 0.246 29.56177 5.81 ug/L Cd 111 79213.299 1.437 0.061 29.21958 4.62 ug/L Cd 114 196073.182 0.596 0.152 32.12405 2.92 ug/L In 115 1291235.816 3.509 1291235.816 ug/L . Sb 121 275140.630 2.981 0.213 31.76944 1.68 ug/L Sb 123 206397.094 0.844 0.160 29.82409 3.75 ug/L Ba 135 80891.112 0.797 0.045 29.87455 2.71 ug/L Ba 137 146932.405 0.909 0.082 30.71607 4.15 ug/L > Tb 159 1791428.528 3.525 1791428.528 ug/L Ho 165 1746222.163 0.635 -0.001 ug/L n 205 746362.598 2.195 0.416 31.72809 1.85 ug/L Pb 208 1014810.051 1.045 0.566 30.83139 2.53 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Se-1 45 101.070 Cr 52 Cr 53 Mn 55

Sample ID: CCV STD1 30PPB Report Date/Time: Tuesday, April 16, 2002 11:25:14 Page 1

NYC-WTC_000040802

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