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ICPMS daily performance check report, April 25, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on April 25, 2002.

NYC-WTC_000053337–000053387

Folder label: “ICPMS 4/25/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08963 Sample Date/Time: Thursday, April 25, 2002 15:07:38 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1 \elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\dataset\newyork city\AE08963.704 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 5.667 26.956 -0.000 -0.00995 43.19 ug/L Se-1 45 456011.800 1.858 456011.800 ug/L Cr 52 8163.412 1.094 0.003 0.13761 18.79 ug/L Cr 53 1235.763 4.045 0.002 0.71492 10.15 ug/L Mn 55 250034.952 1.234 0.545 18.92598 0.91 ug/L Ni 60 901.054 3.847 0.002 0.35632 6.55 ug/L Cu 63 40439.154 1.120 0.088 8.47191 1.61 ug/L Cu 65 19917.662 0.863 0.043 8.42379 1.67 ug/L Zn 66 2086.927 0.402 0.013 0.75089 3.90 ug/L Zn 67 560.023 1.115 0.004 1.38640 4.78 ug/L Zn 68 2147.275 3.223 0.015 1.22675 1.14 ug/L > Ge 72 90768.308 2.485 90768.308 ug/L As 75 785.676 6.603 0.007 0.35824 5.93 ug/L Se 77 168.612 7.896 0.001 0.39130 24.62 ug/L Se 82 139.336 6.669 0.000 0.13462 34.73 ug/L Ag 107 260.340 1.174 0.000 0.01551 1.71 ug/L > in 115 1210604.001 0.318 1210604.001 ug/L Sb 121 578.358 3.978 0.000 0.06796 4.00 ug/L Sb 123 429.791 1.427 0.000 0.06433 1.23 ug/L Ba 135 40796.411 0.710 0.025 16.55669 0.33 ug/L Ba 137 70635.055 0.266 0.043 16.42131 0.77 ug/L Ho 165 1617524.135 0.943 0.000 ug/L > Tb 159 1636034.706 1.017 1636034.706 ug/L Hg 201 48.334 8.362 0.000 0.00612 72.13 ug/L Hg 202 108.668 7.718 0.000 0.01600 20.07 ug/L TI 205 897.387 6.673 -0.000 -0.00420 58.39 ug/L Pb 208 7945.433 0.783 0.004 0.21146 0.44 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 108.744 Cr 52 Cr 53 Mn 55

Sample ID: AE08963 Report Date/Time: Thursday, April 25, 2002 15:09:19 Page 1

NYC-WTC_000053368

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