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ICPMS daily performance check report, May 9, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 9, 2002.

NYC-WTC_000053212–000053335

Folder label: “ICPMS 5/9/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09567 Sample Date/Time: Thursday, May 09, 2002 10:58:15 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09567.855 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 10.000 36.056 -0.000 - -0.00282 294.46 ug/L Li 6 56724.004 1.326 56724.004 mg/L Se-1 45 488570.784 0.908 488570.784 ug/L Cr 52 11711.657 1.317 0.009 0.43666 4.93 ug/L Cr 53 3249.280 3.028 0.005 1.87757 4.53 ug/L Mn 55 914558.150 0.874 1.866 50.77586 1.54 ug/L Ni 60 3054.877 2.235 0.006 1.07637 1.61 ug/L Cu 63 9486.044 2.857 0.019 1.46770 2.36 ug/L Cu 65 4207.349 2.546 0.008 1.30087 3.26 ug/L Zn 66 2551.384 2.242 -0.004 -0.27007 8.10 ug/L Zn 67 810.044 7.164 0.002 0.80084 22.03 ug/L Zn 68 2956.844 2.167 0.005 0.37989 8.46 ug/L Ge 72 119924.882 1.959 119924.882 ug/L As 75 11675.209 1.324 0.012 0.58974 19.35 ug/L Se 77 1628.303 3.151 0.002 1.18914 28.07 ug/L Se 82 -52.142 338.276 0.000 0.08902 720.77 ug/L As-1 75 1706.511 3.210 1463.172 0.57381 3.74 ug/L Kr 83 4155.325 2.030 -238.448 ug/L Ag 107 144.336 14.035 -0.000 -0.00129 110.05 ug/L Cd 111 136.002 18.645 0.000 0.01169 59.36 ug/L Cd 114 418.316 56.429 0.000 0.02804 107.01 ug/L in 115 1685883.909 1.851 1685883.909 ug/L Sb 121 761.373 5.274 0.000 0.06266 6.74 ug/L Sb 123 612.786 4.304 0.000 0.06555 6.67 ug/L Ba 135 103038.846 2.147 0.038 28.20942 2.67 ug/L Ba 137 179655.438 1.243 0.066 28.23463 1.37 ug/L Ho 165 2729269.539 1.771 -0.009 ug/L Tb 159 2701422.783 0.755 2701422.783 ug/L Hg 201 67.334 8.702 0.000 0.00335 100.58 ug/L Hg 202 135.002 9.457 0.000 0.00351 88.18 ug/L TI 205 460.016 10.552 -0.000 -0.01622 7.42 ug/L Pb 208 6079.852 1.208 0.001 0.05694 3.47 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff

Sample ID: AE09567 Report Date/Time: Thursday, May 09, 2002 11:00:08 Page 1

NYC-WTC_000053273

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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