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ICPMS daily performance check report, May 8, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV CAL BK Sample Date/Time: Wednesday, May 08, 2002 10:43:24 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\ICV CAL BK.779 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 12.667 31.906 0.000 ' 0.00280 350.97 ug/L > Se-1 45 504841.779 1.067 504841.779 ug/L Cr 52 8377.287 6.679 0.001 0.03071 184.20 ug/L Cr 53 856.049 1.799 0.000 0.01029 162.89 ug/L Mn 55 6933.380 2.677 0.000 0.00014 6960.31 ug/L Ni 60 82.001 8.449 -0.000 -0.00588 36.01 ug/L Cu 63 234.005 6.453 -0.000 -0.00318 66.57 ug/L Cu 65 189.337 6.367 0.000 0.00245 135.39 ug/L Zn 66 1169.433 49.759 0.003 0.19925 138.93 ug/L Zn 67 184.337 3.488 0.000 0.03527 49.42 ug/L Zn 68 684.033 5.445 0.000 0.03309 79.01 ug/L > Ge 72 126948.857 0.699 126948.857 ug/L As 75 11606.369 0.672 0.002 0.07387 60.57 ug/L Se 77 1514.102 1.827 0.000 0.02140 588.10 ug/L Se 82 -131.504 40.854 -0.001 -0.24087 78.27 ug/L Kr 83 4460.805 0.704 -0.667 ug/L Ag 107 586.025 4.447 0.000 ,0.01031 20.64 ug/L > In 115 1884375.991 1.706 1884375.991 ug/L Sb Sb Ba Ba 121 123 135 137 251.339 209.351 60.334 98.335 12.162 17.913 26.329 20.750 0.801 0.000 0.000 0.000 0.000 J 0.03991 0.01048 0.00'133 0.i.op 105 23.79 32.67 314.10 295.44 ug/L ug/L ug/L ug/L ug/L > Tb 159 2655444.836 2655444.836 Hg 201 140.336 19.804 0.000 0.03930 161.32 ug/L Hg 202 298.675 13.904 0.000 0.00843 115.77 ug/L TI 205 1590.488 1.641 -0.000 -0.00066 91.85 ug/L Pb 208 2959.885 2.946 0.000 0.00095 211.71 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 s Se-1 45 98.725 Cr 52 Cr 53 Mn 55

Sample ID: ICV CAL BK Report Date/Time: Wednesday, May 08, 2002 10:45:57 Page 1

NYC-WTC_000053101

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NYC-WTC_000053101Source: NYC Law Department, mirrored locally

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