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ICPMS daily performance check report, May 3, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV CAL BK Sample Date/Time: Friday, May 03, 2002 10:25:07 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyorkcity\ICV CAL BK.717 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.667 5.413 -0.000' -0.00090 66.77 ug/L > Se-1 45 569787.639 2.385 569787.639 ug/L Cr 52 9326.876 1.499 0.001 0.03050 91.66 ug/L Cr 53 772.374 5.411 -0.000 -0.03887 46.78 ug/L Mn 55 2246.300 0.887 -0.001 -0.01547 22.25 ug/L Ni 60 237.672 6.854 -0.000 -0.00262 157.02 ug/L Cu 63 446.349 7.090 0.000 0.00207 273.39 ug/L Cu 65 236.005 5.509 0.000 0.01228 41.54 ug/L Zn 66 1260.100 6.692 0.000 0.01866 177.58 ug/L Zn 67 255.006 4.242 -0.000 -0.03214 124.43 ug/L Zn 68 961.727 1.249 0.000 0.00605 120.09 ug/L > Ge 72 108015.463 1.836 108015.463 ug/L As 75 8726.739 3.950 0.004 0.21076 80.76 ug/L Se 77 1143.225 2.104 0.000 0.24522 70.82 ug/L Se 82 3293.963 3.279 0.002 0.70609 75.08 ug/L Ag 107 2497.373 15.247 0.002 0.20625 19.56 ug/L Cd 111 60.001 10.138 0.000 0.00044 590.51 ug/L Cd 114 103.035 13.736 -0.000 -0.00551 46.41 ug/L > In 115 1320081.593 1.663 1320081.593 ug/L Sb 121 56.001 5.357 0.000 0.00193 22.71 ug/L Sb 123 37.935 17.552 -0.000 -0.00016 677.68 ug/L Ba 135 49.001 15.408 -0.000 -0.00060 504.48 ug/L Ba 137 87.335 4.628 0.000 0.00159 58.36 ug/L Ho 165 1855984.872 1.172 0.075 ug/L > Tb 159 1807837.901 0.638 1807837.901 ug/L Hg 201 111.668 14.338 0.000 0.04092 33.18 ug/L Hg 202 220.672 17.507 0.000 0.04041 34.85 ug/L TI 205 663.364 4.792 0.000 0.00024 525.88 ug/L Pb 208 1884.761 4.356 -0.000 -0.00296 89.25 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 > Se-1 45 92.965 Cr 52

Sample ID: ICV CAL BK Report Date/Time: Friday, May 03, 2002 10:26:54 Page 1

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