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ICPMS daily performance check report, May 3, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: QCS 50 AND 4 PPB Hg Sample Date/Time: Friday, May 03, 2002 10:44:58 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\QCS 50 AND 4 PPB Hg.721 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 26124.774 3.416 0.048 49.77397 3.83 ug/L Se-1 45 545310.914 0.415 545310.914 ug/L Cr 52 588761.364 1.557 1.064 51.98003 2.00 ug/L Cr 53 66262.278 0.638 0.120 49.94132 0.59 ug/L Mn 55 934608.792 2.105 1.709 51.11890 1.72 ug/L Ni 60 127550.678 2.947 0.233 49.76485 3.34 ug/L Cu 63 278178.907 1.417 0.509 51.46292 1.12 ug/L Cu 65 141847.938 1.277 0.260 51.92506 1.67 ug/L Zn 66 90395.799 0.993 0.838 49.39450 1.31 ug/L Zn 67 16618.008 0.332 0.154 50.34163 0.50 ug/L Zn 68 67086.316 1.255 0.622 49.13286 1.58 ug/L Ge 72 106418.979 0.305 106418.979 ug/L As 75 117164.514 3.113 1.024 50.71835 3.63 ug/L Se 77 10716.298 1.759 0.091 50.12035 2.22 ug/L Se 82 14538.431 1.913 0.108 50.28894 2.74 ug/L Ag 107 564091.884 0.827 0.426 53.80224 1.59 ug/L Cd 111 137725.914 2.602 0.104 50.21884 1.79 ug/L Cd 114 314354.174 0.753 0.237 49.99964 0.96 ug/L > In 115 1324122.675 0.818 1324122.675 ug/L Sb 121 455841.593 0.810 0.344 51.31286 1.53 ug/L Sb 123 345165.548 1.158 0.261 51.19918 0.34 ug/L Ba 135 131611.530 0.886 0.071 49.19930 0.88 ug/L Ba 137 221675.527 1.044 0.120 48.99716 0.64 ug/L Ho 165 1774289.484 1.309 0.009 ug/L Tb 159 1847884.745 0.453 .1847884.745 ug/L Hg 201 5126.830 1.119 0.003 4.02289 1.39 ug/L Hg 202 11714.328 1.714 0.006 3.99276 1.37 ug/L TI 205 1293518.704 0.815 0.700 50.31906 0.42 ug/L Pb 208 1800144.681 0.207 0.973 49.56410 0.66 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff ’ Be 9 > Sc-1 45 88.972 Cr 52

Sample ID: QCS 50 AND 4 PPB Hg Report Date/Time: Friday, May 03, 2002 10:48:14 Page 1

NYC-WTC_000052985

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