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ICPMS daily performance check report, May 9, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 9, 2002.

NYC-WTC_000053212–000053335

Folder label: “ICPMS 5/9/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: QCS 50 AND 4 PPB Sample Date/Time: Thursday, May 09, 2002 09:53:54 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\QCS 50 AND 4 PPB.841 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 21179.193 1.916 0.374 50.03158 2.42 ug/L .> Li 6 56646.854 1.203 56646.854 mg/L > Sc-1 45 514558.692 3.189 514558.692 ug/L Cr 52 570207.480 2.453 1.095 50.98385 5.09 ug/L Cr 53 67802.660 2.157 0.130 49.44813 2.89 ug/L Mn 55 944648.750 2.305 1.830 49.80227 1.49 ug/L Ni 60 147014.115 1.318 0.286 50.16818 3.52 ug/L Cu 63 332962.655 1.484 0.647 50.51106 2.45 ug/L Cu 65 163727.872 1.956 0.318 50.31119 4.83 ug/L ' Zn 66 109958.817 1.107 0.842 50.76326 1.13 ug/L Zn 67 19161.698 0.678 0.147 50.45708 0.41 ug/L Zn 68 82075.346 1.061 0.628 49.77867 1.05 ug/L > Ge 72 126723.728 0.411 126723.728 ug/L As 75 143498.382 2.114 1.047 50.37807 2.50 ug/L Se 77 13705.518 1.992 0.097 49.83657 1.90 ug/L Se 82 14235.159 2.038 0.113 49.02125 1.68 ug/L As-1 75 128057.955 2.568 127814.615 50.12482 2.57 ug/L Kr 83 4280.717 0.449 -113.055 ug/L Ag 107 772576.953 0.769 0.426 51.96163 1.72 ug/L Cd 111 187757.971 1.661 0.104 49.45084 0.40 ug/L Cd 114 442024.621 1.165 0.244 50.02783 1.37 ug/L > In 115 1812747.478 2.025 1812747.478 ug/L Sb 121 621371.874 1.758 0.343 51.26551 0.74 ug/L Sb 123 476706.234 1.027 0.263 51.11259 0.99 ug/L Ba 135 180365.280 1.186 0.066 48.70864 0.31 ug/L Ba 137 315031.830 1.268 0.115 48.84422 1.73 ug/L Ho 165 2773517.624 0.463 -0.007 ug/L > Tb 159 2739065.209 1.233 2739065.209 ug/L Hg 201 7185.577 0.991 0.003 3.87675 0.97 ug/L Hg 202 16289.745 0.971 0.006 3.87976 2.17 ug/L n 205 2068911.928 5.928 0.755 48.77454 6.70 ug/L Pb 208 2633559.711 1.127 0.960 48.40340 1.72 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff

Sample ID: QCS 50AND4PPB Report Date/Time: Thursday, May 09, 2002 10:00:32 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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