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ICPMS daily performance check report, May 3, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: CCV STD2 60 AND 5 Hg Sample Date/Time: Friday, May 03, 2002 16:52:30 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\CCV STD2 60 AND 5 Hg.755 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 29758.266 1.697 0.066 68.10968 1.79 ug/L Sc-1 45 454125.323 3.511 454125.323 ug/L Cr 52 565870.712 0.751 1.231 60.16376 4.13 ug/L Cr 53 64839.286 6.102 0.141 58.76223 3.59 ug/L Mn 55 909266.573 0.577 1.999 59.79322 3.57 ug/L Ni 60 134801.571 3.556 0.296 63.18542 2.51 ug/L Cu 63 273292.787 1.636 0.601 60.75306 1.96 ug/L Cu 65 141270.823 1.773 0.311 62.17672 4.85 ug/L Zn 66 91103.727 2.995 1.020 60.13098 4.24 ug/L Zn 67 16563.913 2.231 0.185 60.61169 2.39 ug/L Zn 68 70459.495 2.700 0.789 62.36830 4.04 ug/L > Ge 72 88344.474 1.644 88344.474 ug/L As 75 119199.695 0.978 1.273 63.01881 2.05 ug/L Se 77 10559.348 4.595 0.109 60.56404 5.98 ug/L Se 82 14675.660 3.653 0.137 64.10986 6.06 ug/L Ag 107 524427.991 1.315 0.439 55.46574 1.37 ug/L Cd 111 145874.054 2.720 0.122 58.99985 3.18 ug/L Cd 114 323560.267 2.328 0.271 57.07534 2.64 ug/L In 115 1194066.203 1.032 1194066.203 ug/L Sb 121 475378.164 2.307 0.398 59.34429 2.85 ug/L Sb 123 374370.572 2.457 0.314 61.59266 3.20 ug/L Ba 135 139740.886 0.402 0.084 58.20434 1.76 ug/L Ba 137 235349.779 3.169 0.142 57.97579 4.49 ug/L Ho 165 1668202.123 3.699 0.055 ug/L > Tb 159 1658840.855 1.452 1658840.855 ug/L Hg 201 5722.191 1.969 0.003 5.01528 3.34 ug/L Hg 202 13734.838 0.426 0.008 5.22738 1.79 ug/L Tl 205 1420431.831 1.747 0.856 61.57475 2.89 ug/L Pb 208 1976128.303 0.380 1.190 60.62858 1.26 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 74.094 Cr 52

Sample ID: CCV STD2 60 AND 5 Hg Report Date/Time: Friday, May 03, 2002 16:54:58 Page 1

NYC-WTC_000053087

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