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GCMS analysis results for sample AE01222, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01222 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052824–000052831

Folder label: “GCMS X 1/17/02 A 2/16/02

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NYC 9/11 Public Portal Document LOU ALtc rtLCEtit REpOL L

Data File : C:\HPCHEM\l\DATA\FEB1502\1222.D Vial: 28 ' Acq On : 16 Feb 2002 7:34 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.335 788 794 809 rVB 705599 1640740 74.30% 15.198% 2 15.971 1184 1190 1202 rBV 998287 1973588 89.38% 18.281% 3 21.286 1763 1769 1784 rBV 1135514 2208169 100.00% 20.454% 4 25.738 2247 2254 2265 rBV 1040818 2110158 95.56% 19.546% 5 30.815 2802 2807 2813 rVB 131710 245099 11.10% 2.270% 6 33.799 3126 3132 3145 rBV 657593 1488059 67.39% 13.784% 7 38.086 3591 3599 3626 rBV2 377635 1130043 51.18% 10.467%

Sum of corrected areas: 10795856

1222.D GCMS0208.M Wed Feb 20 14:30:03 2002

NYC-WTC_000052829

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NYC-WTC_000052829Source: NYC Law Department, mirrored locally

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