Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
NYC-WTC_000052630–000052637Folder label: “GCMS X 1/15/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\l\DATA\FEB1402\1045.D Vial: 8 Acq On 14 Feb 2002 4:52 pm Operator: 209 GALOS Sample GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 12:51 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 326167 20.00 ug/1 0.00 10) Naphthalene-d8 15.98 136 1260362 20.00 ug/1 -0.01 17) Acenaphthene-dlO 21.30 164 677963 20.00 ug/1 -0.01 29) Phenanthrene-diO 25.75 188 1015628 20.00 ug/1 -0.01 38) Chrysene-dl2 33.82 240 725511 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 450460 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.83 235 57099 5.60 ug/mL 0.33 Spiked Amount 5.000 Recovery = 112.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 624 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.83 152 948 N.D. 2 3) Acenaphthene 21.39 153 1192 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.78 149 500 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.92 166 2576 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1045.D GCMS0308.M Thu Mar 14 15:24:37 2002 Page 1
NYC-WTC_000052630
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NYC-WTC_000052600
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052644
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052884
Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052707
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052666
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052614
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052832
GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009650
Calibration table page listing internal standards and response factors for GCMS analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006371
Initial GCMS analysis report for sample AE01940 conducted by analyst DLV on March 13, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016118
Calibration table for GCMS analysis listing surrogate compounds and response factors from January 16, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006387
Calibration table listing retention times and responses for deuterated standards including naphthalene-d8.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058798
Laboratory report page showing surrogate recovery data for sample AE01153 analyzed on March 22, 2002.
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