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GCMS calibration table for TCLP analysis, February 2002

Machine-extracted title · confidence 100%

Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052630–000052637

Folder label: “GCMS X 1/15/02 A 2/28/02

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NYC 9/11 Public Portal Document uai:t — CO — -11 ISPUL VL ACVACWC)

Data File : C:\HPCHEM\l\DATA\FEB1402\1045.D Vial: 8 Acq On : 14 Feb 2002 4:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 12:51 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.82 178 8262 N.D. 34) Anthracene 25.95 178 5924 N.D. 35) Di-n-butylphthalate 27.72 149 3536 N.D. 36) Fluoranthene 29.44 202 14414 N.D. 39) Pyrene 30.12 202 14904 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.77 228 2119 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 1533 N.D. 43) Chrysene 33.90 228 963 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.89 252 1132 N.D. 47) Benzo(k)fluoranthene 36.89 252 2014 N.D. 48) Benzo(a)pyrene 37.91 252 550 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1045.D GCMS0308.M Thu Mar 14 15:24:41 2002 Page 2

NYC-WTC_000052631

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NYC-WTC_000052631Source: NYC Law Department, mirrored locally

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