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GCMS calibration data review for Method 508, Feb 2002

Machine-extracted title · confidence 90%

Reviewed calibration data sheet for GCMS Method 508 listing retention times and concentrations for deuterated internal standards.

NYC-WTC_000052361–000052363

Folder label: “GCMS X 1/14/02 A 2/22 - 2/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\0 2 2 2 0 2\CAL4 0.D Vial: 17 Acq On : 23 Feb 2002 2:06 am Operator: McLean Sample : 1/14/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Feb 25 19:18:49 2002 Quant Results File: 5080202.RES

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

47) Benzo (k) fluoranthene 33.37 252 4232079 38.81 ug/L 99 48) Benzo (a) pyrene 34.09 252 3701580 39.03 ug/L 98 49) Indeno (1,2,3-cd) pyrene 36.78 276 2735755 39.85 ug/L 98 50) Dibenz (a,h) anthracene 36.89 278 2691036 38.99 ug/L 99 51) Benzo (g,h,i) perylene 37.47 276 2744282 39.74 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL40.D 5080202.M Wed Feb 2 7 06:27:04 2 0 02 Page 2

NYC-WTC_000052362

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NYC-WTC_000052362Source: NYC Law Department, mirrored locally

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