Laboratory report detailing GCMS analysis results for sample AE00943 listing concentrations of volatile organic compounds.
NYC-WTC_000052357–000052360Folder label: “GCMS X 1/14/02 A 2/22 - 2/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\l\DATA\022202\CALX25.D Vial: 2 . Acq On 22 Feb 2002 11:24 am Operator: McLean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Feb 25 19:18:00 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.58 150 1110706 20.00 ug/L 0.00 10) Naphthalene-d8 13.06 136 2673896 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.17 164 1396770 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.53 188 2253277 20.00 ug/L 0.00 38) Chrysene-dl2 30.36 240 2050961 20.00 ug/L 0.00 44) Perylene-dl2 34.22 264 1430543 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.46 235 22348 0.62 ug/L 0.00 Spiked Amount 5.000 Recovery = 12.40%
Target Compounds 14/322 Qvalue 2) N-nitroso-dimethyl amine 3.57 74 820265 24.42 ug/L 100 3) bis(2-chloroethyl) ether 9.03 93 1310597 24.92 ug/L. 98 4) 1,3 - Dichlorobenze 9.42 146 1238076 24.93 ug/L 99 5) 1,4 - Dichlorobenzene 9.62 146 1236749 25.06 ug/L 98 6) 1,2 - Dichlorobenzene 10.01 146 1155984 25.30 ug/L 100 7) 2,2 1 - oxybis (l-Chloropr 10.47 45 3105216 24.42 ug/L 99 8) N-Nitroso-di-n-propylamine 10.82 70 1036502 25.69 ug/L 98 9) Hexachloroethane 10.89 117 491004 24.61 ug/L 96 11) Nitrobenzene 11.16 77 1544607 24.78 ug/L 98 12) Isophorone 11.87 82 2787736 24.52 ug/L 99 13) bis(2-Chloroethoxy) methan 12.60 93 1716021 24.90 ug/L 100 14) 1,2,4-Trichlorobenzene 12.94 180 983301 25.86 ug/L 98 15) Naphthalene 13.13 128 3521394 25.04 ug/L 100 16) Hexachlorobutadiene 13.57 225 549061 26.00 ug/L 99 18) Hexachlorocyclopentadiene 15.64 237 342702 25.09 ug/L 99 19) 2-chloronaphthalene 16.55 162 2062824 25.84 ug/L 99 20) Dimethylphthalate 17.64 163 2455766 25.79 ug/L 98 21) 2,6-Dinitrotoluene 17.75 165 499866 25.72 ug/L 99 22) Acenaphthylene 17.73 152 2831037 25.80 ug/L 99 23) Acenaphthene 18.27 153 1965865 25.79 ug/L 99 24) 2,4-Dinitrotoluene 18.90 165 739930 26.52 ug/L 97 25) Diethylphthalate 19.79 149 2175504 26.67 ug/L 100 26) 4-Chlorophenyl-phenyl ethe 19.94 204 1123673 26.49 ug/L 100 27) Fluorene 19.80 166 2261963 26.04 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.40 77 3144289 25.23 ug/L 99 30) N-Nitrosodiphenylamine 20.32 169 1550927 25.79 ug/L 99 31) 4-Bromophenyl-phenyl ether 21.36 248 643906 27.06 ug/L 97 32) Hexachlorobenzene 21.39 284 652540 26.65 ug/L 98 33) Phenanthrene 22.60 178 3315682 25.38 ug/L 99 34) Anthracene 22.75 178 3140270 25.04 ug/L 100 35) Di-n-butylphthalate 24.69 149 3990502 26.44 ug/L 100 36) Fluoranthene 26.11 202 3855526 25.65 ug/L 98 39) Pyrene 26.74 202 3998536 23.99 ug/L 96 40) Butylbenzylphthalate 29.09 149 1800099 25.21 ug/L 92 41) Benzo (a) antracene 30.32 228 3346008 24.87 ug/L 100 42) Bis (2-ethylhexyl) phthala 30.95 149 2416535 25.98 ug/L 98 43) Chrysene 30.43 228 3194035 24.35 ug/L 99 45) Di-n-Octylphthalate 32.80 149 4084351 27.84 ug/L 99 46) Benzo (b) fluoranthene 33.28 252 3088897 25.81 ug/L 99
(#) = qualifier out of range (m) = manual integration CALX25.D 5080202.M Wed Feb 27 06:14:01 2002 Page 1
NYC-WTC_000052358
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NYC-WTC_000052424
Gas chromatography-mass spectrometry calibration results for sample AE01641 analyzing volatile organic compounds in March 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010469
Laboratory analysis report for sample AE02152 conducted on March 18, 2002, listing volatile organic compounds.
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Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
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Laboratory form detailing analytical methods and parameters including drip rate and pH for a sample analyzed on March 19, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011057
Calibration data report for sample AE03075 showing response values for multiple organic compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039116
GCMS calibration report for sample AE05902 listing response factors and retention times for multiple compounds on March 20, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011206
Laboratory report showing GCMS detection of multiple volatile organic compounds in environmental sample AE03253 on April 2, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039120
GCMS reference analysis report for sample AE05902 listing quantitative results for multiple volatile organic compounds on March 20, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012416
Laboratory report showing gas chromatography mass spectrometry results for sample AE04337 analyzed on March 27, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012094
Calibration data for sample AE01639 verifying instrument performance for volatile organic compound analysis on March 21, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011611
Reference standard response values for GC/MS analysis conducted on March 15, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039213
GCMS calibration results for sample AE06267 showing quantified organic compounds including nitrosamines and chlorinated solvents.
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NYC-WTC_000052330
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NYC-WTC_000052331
Document header or log entry indicating GCMS analysis activities conducted between February 22 and 23, 2002.
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NYC-WTC_000052332
Technical data sheet recording GCMS Method 508 calibration results including response factors and percent relative standard deviation for various compounds.
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NYC-WTC_000052355
Quality control report verifying GCMS performance using DFTPP standards with pass/fail status for specific mass fragments.
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Reviewed calibration data sheet for GCMS Method 508 listing retention times and concentrations for deuterated internal standards.
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