GCMS method 508 calibration data sheet, Feb 2002

NYC 9/11 Public Portal Document

Response Factor Report Instrumen

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration

Calibration Files 6 =CAL6.D 1 =CAL1.D 2 =CAL2.D 3 =CAL3.D 4 =CAL4.D 5 =CAL5.D

Compound 6 1 2 3 4 5 Avg %RSD

1) I 1,4-Dichlorobenzene-d I STD 2) T N-nitroso-dimet 0.565 0.639 0.659 0.619 0.565 0.583 0.605 6.57 3) bis(2-chloroeth 0.827 1.196 1.112 0.922 0.817 0.807 0.947 17.74 4) 1,3 Dichlorob 0.773 1.090 1.034 0.890 0.793 0.785 0.894 15.36 5) 1,4 Dichlorob 0.754 1.090 1.044 0.883 0.794 0.766 0.888 16.47 6) 1,2 Dichlorob 0.703 1.034 0.958 0.816 0.723 0.702 0.823 17.34 7) 2,2 ‘ - oxybis 1.897 2.905 2.681 2.294 2.016 1.948 2.290 18.29 8) N-Nitroso-di-n- 0.838 0.850 0.752 0.648 0.543 0.726 17.96 9) I Hexachloroethan 0.429 0.420 0.361 0.318 0.269 0.359 18.86

10) Naphthalene-d8 ------------------------------- ISTD---------------------------------- 11) Nitrobenzene 0.420 0.526 0.506 0.467 0.441 0.437 0.466 8.98 12) Isophorone 0.812 0.905 0.899 0.847 0.804 0.835 0.850 5.04 13) bis(2-Chloroeth 0.462 0.583 0.574 0.516 0.483 0.474 0.515 10.08 14) 1,2,4-Trichloro 0.245 0.330 0.320 0.290 0.269 0.253 0.284 12.31 15) Naphthalene 0.877 1.266 1.213 1.055 0.982 0.918 1.052 15.05 16) Hexachlorobutad 0.134 0.186 0.179 0.159 0.150 0.139 0.158 13.41

17) Acenaphthene-diO --------------- ISTD----------------- 18) Hexachlorocyclo 0.213 0.136 0.165 0.215 0.220 0.224 0.196 18.68 19) T 2-chloronaphtha 0.934 1.338 1.305 1.172 1.107 1.000 1.143 14.14 20) 1 Dimethylphthala 1.185 1.488 1.491 1.404 1.350 1.261 1.363 9.03 21) T 2,6-Dinitrotolu 0.264 0.268 0.291 0.292 0.281 0.274 0.278 4.16 22) Acenaphthylene 1.285 1.825 1.788 1.611 1.534 1.385 1.571 13.68 23) Acenaphthene 0.885 1.324 1.231 1.105 1.049 0.955 1.092 15.16 24) 2,4-Dinitrotolu 0.381 0.365 0.414 0.423 0.414 0.399 0.399 5.56 25) Diethylphthalat 0.885 1.424 1.346 1.231 1.164 0.959 1.168 18.17 26) 4-Chlorophenyl- 0.506 0.705 0.675 0.632 0.591 0.535 0.607 12.88 27) Fluorene 0.960 1.546 1.471 1.260 1.203 1.024 1.244 18.83 28) Azobenzen/ 1,2- 1.537 2.020 1.942 1.823 1.717 1.667 1.784 10.07

29) Phenanthrene-dl0 ------------------------------- ISTD---------------------------------- 30) N-Nitrosodiphen 0.441 0.634 0.614 0.546 0.508 0.460 0.534 14.81 31) 4-Bromophenyl-p 0.171 0.250 0.245 0.217 0.204 0.180 0.211 15.41 32) Hexachlorobenze 0.182 0.260 0.247 0.220 0.206 0.189 0.217 14.38 33) Phenanthrene 0.963 1.416 1.334 1.168 1.087 0.989 1.159 15.87 34) Anthracene 0.923 1.325 1.288 1.123 1.054 0.964 1.113 14.89 35) Di-n-butylphtha 1.128 1.513 1.527 1.391 1.313 1.167 1.340 12.63 36) Fluoranthene 1.139 1.547 1.499 1.353 1.282 1.183 1.334 12.37 37) s 2,4-ddd surr 0.318 0.318 0.00

38) Chrysene-dl2 ------------------------------- ISTD---------------------------------- 39) Pyrene 1.576 1.763 1.719 1.603 1.553 1.538 1.625 5.76 40) Butylbenzylphth 0.706 0.622 0.705 0.733 0.706 0.705 0.696 5.48 41) Benzo (a) antra 1.290 1.318 1.355 1.328 1.291 1.291 1.312 2.03 42) Bis (2-ethylhex 0.887 0.820 0.947 0.967 0.926 0.895 0.907 5.77 43) Chrysene 1.167 1.451 1.397 1.262 1.215 1.182 1.279 9.25 44) Perylene-d12 --------------- ISTD----------------- 45) Di-n-Octylphtha 2.102 1.604 2.000 2.269 2.247 2.083 2.051 11.79 46) Benzo (b) fluor 1.667 1.693 1.720 1.671 1.663 1.625 1.673 1.90 47) Benzo (k) fluor 1.532 1.896 1.868 1.716 1.680 1.525 1.703 9.33

ft) = Out of Range 5080202.M Wed Feb 27 08:07:43 2002 Page 1

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