GCMS analysis results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00842 .D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 4-Penten-2-one Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.77 0.10 ug/L 39480 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Penten-2-one 84 C5H80 013891-87-7 3 2 Ethanol-D5 51 C2HD50 000000-00-0 3 3 4-Penten-2-one $$ Allyl methyl k... 84 C5H80 013891-87-7 3 4 4-Penten-2-one (CAS) $$ Methyl a... 84 C5H80 013891-87-7 3 Abundance Scan 35 (3.773 min): 00842.D (-) m/z 43.10 100.00% 43

5000

Of ■ । ■' ■ ■ ।' ■' ■ ।' mm —H 36 51 r ■' ■ i ■'' ■ i 84 I " " 11" 11"111" A m/ z 3.60 1 3.80 84.00 4.00 4.20 10.09% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3242:4-Penten-2-one 43

5000 3.60 3.80 4.00 4.20 m/z 51.10 9.90% 39 84

m/z-> Abundance 0- ‘T‘ i ■ ■ ‘ ■ i +t .......... i > • • ■ i ■i•■> ■ i — 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90

33 #311: Ethanol-D5 AAMA ■ i ■ ■ • ■ i ■

3.60 3.80 4.00 4.20 5000 m/z 36.10 7.73%

26 i 30 46 52 49 1 N

n/z-> Or 5 Th" 10 I" " IT’T +t ।........ # | •1 ■ ■ l <11' i' ■ ■ ■ i • ■ ■ • i • ■ ■ ■ i 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 11 " ' I'1111"

Abundance #3241:4-Penten-2-one $$ Allyl methyl ketone $$ Methyl all... 43 _______ 380 3.60 4.00 4.20 m/z 49.05 6.09%

5000

15 39 MA„M"ra 27 | 53 69 84 Or ................ ............. i ■' ■ ■ । — . ...... I /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 3.60 3.80 4.00 4.20

00842.D HP020702.M Thu Feb 21 09:58:08 2002 Page 5

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