GCMS blank results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02 FEB 07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 N-(2,3,5-triazolyl)-acetamide Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

11.09 0.10 ug/L 34554 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2,3,5-triazolyl)-acetamide 126 C4H6N4O 000000-00-0 9 2 1H-1,2,4-Triazol-5-amine, 1-prop... 126 C5H10N4 058661-96-4 9 3 2-Cyclobuten-l-one, 3-(acetyloxy... 126 C6H603 038425-52-4 9 4 3 -ACETAMIDO-1,2,4-TRIAZOLE 126 C4H6N40 000000-00-0 9 Abundance Scan 676 (11.091 min): 0111 BA.D (-) m/ z 84.05 100.00% 84 42 126 5000

58 107 141 AWW10.80 11.00 11.20 11.40 ......... I 01 1 i ■ ■ ■ ■ i 1 ' ■ 'i1 • ■ i ■ ■ I ' 1 ' ' I ■ ' ' ' I ' ' "T‘ i i | I i | i | | । i i | UTf i |-r m/z 42.10 72.74% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #22037: N-(2,3,5-triazolyl)-acetamide 84 43

5000 57 10.80 1100 11.20 1140 m/z 126.10 52.96% 126

n/z-> 0 20 235.1 'I50111160111 69 30 40 70 80 ■'i ■'1 ' i 1 90 100 110 120 130 140 TT

Abundance #22142: 1H-1,2,4-Triazol-5-amine, 1-propyl- $$ 1H-1,2,4-Tr... 84 TTT 10.80 11.00 11.20 11.40 5000 97 m/ z 44.20 37.96% 126 55 70 43

mlz—> O' । 1 1 1 1 | ' 20 30 nil 40 ..... 50 TT 60 111'1113 • ■ i ■ 70 80 90 100 110 120 i 1 i r ■ ■ 1 i 1 r ■ ' i 130 140 Abundance #22178: 2-Cyclobuten-1-one, 3-(acetyloxy)- (CAS) 38 45 — 84 10.80 11.00 11.20 11.40 60 126 m/ z 41.00 26.14% A 5000 67

O'' | " " | 'T । | ' 1 । ■ I 1 1 1 1 I 1 ■ 1 । ■ ■ • ■ । ■ ■ ■ ■ । । ' m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 10.80 11.00 11.20 11.40

0111BA.D HP020702.M Thu Feb 21 09:58:24 2002 Page 8

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