GCMS analysis results for sample AE00838, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052167–000052186

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00838.D Vial: 2 Acq On : 31 Jan 2002 3:32 pm Operator: Sample : 508 scan Inst Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 13 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.36 ug/L 309779 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 78 3 8-amino-6-methoxy-2-methylquinoline 188 C11H12N20 000000-00-0 50 4 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H12O2 055139-53-2 49 Abundance Scan 1699 (22.771 min): 00838. D (-) m/z 188.15 100.00% 188

5000

80 94 _| ' ■ • • । • r. r, ' । i > । । > > > । । 22.40 22.60 22.80 23.00 23.20

n/z-> 42 52 66 0 PT 11 > 111111 l 111111 f - —130,146 14010 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 21.75% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 TF । ■ ■ i 1 1 1 1 ।1 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.10 19.55%

n/z-> o 66 ■ । ■ ■ • ■ । ■1 ■ । ■ i • । ■ TtT 158 —ott mIPPPmmTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 l Abundance #84502: Anthracene-d10- 188 / I 1 ' TT 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 17.88%

„ 80 94 160 66 । । 1 0 1' I'' .. . ........... I. ।|111।. ........ . । ।111111111 m । niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #97930:8-amino-6-methoxy-2-methylquinoline ............ 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.27%

5000 159 145

m-> r ■ " i ■■ ■■i•'■' i'1 " i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i' ■1 ■ i T 111113 ■ i ’ ■ ■ ■ । ■ 1 । ■ ■ ■ • । 1 ■ ■ ■ । ’ 22.40 22.60 22.80 23.00 23.20

00838.D SCAN508.M Fri Feb 01 09:19:07 2002 Page 15

NYC-WTC_000052185

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GCMS analysis results for sample AE00839, Feb 4 2002 · Box DEP Box 28

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Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

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