GCMS reference results for sample AE00330, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN31\0111R.D Vial: 2 Acq On : 31 Jan 2002 11:21 am Operator: Sample : ref 1/11 Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 01 08:46:18 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1759299 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 7524463 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 3906294 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 6248295 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 5163638 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3767972 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 399733 4.05 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.00%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 441019 5.88 ug/L # 47 3) bis(2-Chloroethyl)ether 9.24 93 662305 5.57 ug/L 68 4) 1,3-Dichlorobenzene 9.61 146 446474 3.38 ug/L 95 5) 1,4-Dichlorobenzene 9.76 146 462540 3.49 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 457202 3.88 ug/L 96 7) 2,2'-oxybis (l-Chloropropa 10.67 45 861288 4.23 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.05 70 398710 4.29 ug/L 77 9) Hexachloroethane 11.03 117 122206 2.57 ug/L 94 11) Nitrobenzene 11.35 77 554538 3.95 ug/L 80 12) Isophorone 12.02 82 1074939 4.24 ug/L 94 13) bis(2-Chloroethoxy)methane 12.77 93 706795 4.69 ug/L 90 14) 1,2,4-Trichlorobenzene 13.11 180 315681 3.22 ug/L 98 15) Naphthalene 13.25 128 1486919 4.13 ug/L 99 16) Hexachlorobutadiene 13.84 225 118734 2.28 ug/L 96 18) Hexachlorocyclopentadiene 15.96 237 21126 0.61 ug/L 94 19) 2-Chloronaphthalene 16.65 162 731689 3.39 ug/L 93 20) Dimethylphthalate 17.88 163 1005388 3.90 ug/L 94 21) 2,6-Dinitrotoluene 18.06 165 168130 3.34 ug/L 79 22) Acenaphthylene 17.86 152 1193106 3.79 ug/L 97 23) Acenaphthene 18.42 153 832230 3.71 ug/L 98 24) 2,4-Dinitrotoluene 19.17 165 206593 3.14 ug/L 89 25) Diethylphthalate 20.00 149 980795 3.97 ug/L 98 26) 4-Chlorophenyl-phenylether 20.02 204 381260 3.67 ug/L 88 27) Fluorene 19.91 166 967640 3.80 ug/L 97 28) Azobenzene/1,2-Diphenylhyd 20.46 77 1097169 3.56 ug/L 81 30) N-nitrosodiphenylamine 20.42 169 557859 3.52 ug/L 97 31) 4-Bromophenyl-phenylether 21.44 248 219735 3.38 ug/L 90 32) Hexachlorobenzene 21.77 284 214417 3.12 ug/L 99 33) Phenanthrene 22.69 178 1412093 4.10 ug/L 99 34) Anthracene 22.82 178 1267560 3.79 ug/L 99

(#) = qualifier out of range (m) = manual integration 0111R.D SCAN508.M Fri Feb 01 08:46:19 2002 Page 1

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