GCMS reference scan results for sample AD31647, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

•* Data File : C:\MSDCHEM\1\5973N\02JAN22\0103RA.D Vial: 2 Acq On' : 22 Jan 2002 11:21 am Operator: Sample : ref 1/3 a Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 15:30:22 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1234751 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 5192557 20.00 ug/L -0.02 17) Acenaphthene-dl0 18.34 164 2705404 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4613176 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4168547 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3154993 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 377166 5.17 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.40%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 142564 2.71 ug/L 51 3) bis(2-Chloroethyl)ether 9.24 93 369305 4.34 ug/L 68 4) 1,3-Dichlorobenzene 9.61 146 271189 2.93 ug/L 96 5) 1,4-Dichlorobenzene ‘ 9.76 146 283642 3.05 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 285227 3.45 ug/L 99 7) 2,2'-oxybis (1-Chloropropa 10.67 45 522011 3.66 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.05 70 244924 3.76 ug/L 77 9) Hexachloroethane 11.03 117 68327 2.05 ug/L 97 11) Nitrobenzene 11.35 77 303659 3.13 ug/L 83 12) 1sophorone 12.02 82 678537 3.88 ug/L 94 13) bis(2-Chloroethoxy)methane 12.77 93 448726 4.32 ug/L 92 14) 1,2,4-Trichiorobenzene 13.11 180 230726 3.41 ug/L 95 15) Naphthalene 13.25 128 1036784 4.17 ug/L 98 16) Hexachlorobutadiene 13.84 225 65612 1.82 ug/L 96 18) Hexachlorocyclopentadiene 15.95 237 10163 0.42 ug/L 84 19) 2-Chloronaphthalene 16.65 162 584773 3.91 ug/L 92 20) Dimethylphthalate 17.88 163 742690 4.16 ug/L 92 21) 2,6-Dinitrotoluene 18.06 165 102286 2.94 ug/L 79 22) Acenaphthylene 17.86 152 922274 4.23 ug/L 98 2 3) Acenaphthene 18.42 153 667536 4.30 ug/L 99 24) 2,4-Dinitrotoluene 19.17 165 131275 2.88 ug/L 90 25) Diethylphthalate 20.00 149 785200 4.59 ug/L 98 26) 4-Chlorophenyl-phenylether 20.02 204 347176 4.83 ug/L 86 2 7) Fluorene 19.91 166 790753 4.48 ug/L 99 28) Azobenzene/1,2-Diphenylhyd 20.46 77 852563 3.99 ug/L 83 30) N-nitrosodiphenylamine 20.43 169 412656 3.53 ug/L 96 31) 4-Bromophenyl-phenylether 21.44 248 207401 4.32 ug/L 88 32) Hexachlorobenzene 21.77 284 213551 4.21 ug/L 99 3 3) Phenanthrene 22.70 178 1226948 4.83 ug/L 99 34) Anthracene 22.82 178 1163624 4.72 ug/L 98 (#) = qualifier out of range (m) = manual integration 0103RA.D SCAN508.M Tue Jan 22 15:30:23 2002 Page 1

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