GCMS reference calculation sheet for sample AE00314, Jan 15 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN14\0108RA.D Vial: 2 Acq On : 14 Jan 2002 11:18 am Operator: Sample : ref 1/8 a Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 08:47:08 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 981943 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4282625 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2293484 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 3968310 20.00 ug/L -0.03 38) Chrysene-dl2 30.50 240 3575005 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2648443 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 309273 4.93 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.60%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 135352 3.23 ug/L 48 3) bis(2-Chloroethyl)ether 9.24 93 317352 4.72 ug/L 70 4) 1,3-Dichlorobenzene 9.61 146 221219 3.00 ug/L 95 5) 1,4-Dichlorobenzene 9.76 146 230879 3.12 ug/L 95 6) 1,2-Dichlorobenzene 10.24 146 237676 3.62 ug/L 99 7) 2,2'-oxybis (1-Chloropropa 10.68 45 464742 4.09 ug/L # 74 8) n-Nitroso-di-n-propylamine 11.06 70 221932 4.28 ug/L 76 9) Hexachloroethane 11.03 117 53067 2.00 ug/L 95 11) Nitrobenzene 11.35 77 245937 3.08 ug/L 85 12) 1sophorone 12.03 82 624383 4.33 ug/L 92 13) bis(2-Chloroethoxy)methane 12.77 93 409823 4.78 ug/L 92 14) 1,2,4-Trichlorobenzene 13.11 180 197594 3.54 ug/L 96 15) Naphthalene 13.25 128 925856 4.51 ug/L 98 16) Hexachlorobutadiene 13.84 225 63700 2.15 ug/L 99 18) Hexachlorocyclopentadiene 15.96 237 7826 0.38 ug/L # 75 19) 2-Chloronaphthalene 16.65 162 549796 4.34 ug/L 93 20) Dimethylphthalate 17.88 163 735188 4.85 ug/L 95 21) 2,6-Dinitrotoluene 18.06 165 71630 2.42 ug/L 83 22) Acenaphthylene 17.86 152 883263 4.78 ug/L 98 2 3) Acenaphthene 18.42 153 641038 4.87 ug/L 98 24) 2,4-Dinitrotoluene 19.17 165 89885 2.32 ug/L 95 25) Diethylphthalate 20.00 149 764423 5.27 ug/L 97 26) 4-Chlorophenyl-phenylether 20.03 204 338974 5.56 ug/L 80 27) Fluorene 19.91 166 764878 5.11 ug/L 97 28) Azobenzene/1,2-Diphenylhyd 20.46 77 848859 4.69 ug/L 85 30) N-nitrosodiphenylamine 20.43 169 471130 4.68 ug/L 97 31) 4-Bromophenyl-phenylether 21.44 248 201015 4.87 ug/L 90 32) Hexachlorobenzene 21.77 284 210369 4.82 ug/L 99 3 3) Phenanthrene 22.69 178 1201550 5.49 ug/L 99 34) Anthracene 22.82 178 1120657 5.28 ug/L 97

(#) = qualifier out of range (m) = manual integration 0108RA.D SCAN508.M Tue Jan 15 08:47:09 2002 Page 1

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