GCMS results for sample AE00740, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN16\00740.D Vial: 8 Acq On : 16 Jan 2002 8:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 1 2-Pentenal, (E)- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

4.83 0.17 ug/L 66631 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm ’ CAS# Qual

1 2-Pentenal, (E)- 84 C5H80 001576-87-0 17 2 2-Pentyn-l-ol 84 C5H80 006261-22-9 12 3 2-Pentyn-l-ol 84 C5H80 006261-22-9 9 4 Cyclobut-l-enylmethanol 84 C5H80 000000-00-0 9 Abundance Scan 128 (4.835 min): 00740.D (-) m/ z 84.05 100.00% 59 84 55 41 5000

4.40 4.60 4.80 5.00 5.20 Ot ■ i ■' ■ • 11 ‘ • i ■ i'' ■ ■ i ■ ■ ■ • i • ■ ■ ■ i • ■ ■ ■ i ■' m/z 59.10 88.24% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3201:2-Pentenal, (E)- 55 27 39 84 5000 4.40 — A-. -4— -A 4.60 4.80 5.00 5.20 m/z 55.10 72.50% 51

n/z-> O+ — ■' । ■ 35 .... IM. 20 25 30 35 40 45 50 55 66 IIT-ITRTTT i • •'' i ■ ■ 60 65 70 75 80 85 90 Abundance #3292: 2-Pentyn-1-ol 39 ...A 4.40 4.60 4.80 5.00 5.20 83 m/z 41.10 52.50% 5000 27 51 65« I..,70...75 - rn/z-> Abundance 01 • i • • ■ > i ■ 20 25 ■ i ■ • • ■ i ■ 30 35 40

39 45 50 55 60 65 TTT

#3291:2-Pentyn-1-ol 55 80 85 90 A 4.40 m/ z A. N 4.60 39.10 4.80 —A 5.00 5.20 49.76% 83 5000 27

44 51 66

n/z-> 01 ‘1211111 - 20 25 30 35 40 -44- 45 50 55 60 65 70 75 80 11 ■' •' i ■ • 85 90 4.40 4.60 4 80 5.00 5.20

)0740.D SCAN508.M Thu Jan 17 08:17:57 2002 Page 3

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