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GCMS results for sample AE00739, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051967–000051983

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

W—W/

Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 ' Acq Ori : 16 Jan 2002 8:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 17 08:12:25 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1300604 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 5588695 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2912323 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4760249 20.00 ug/L -0.02 38) Chrysene-dl2 30.49 240 4024900 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2952703 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 385930 5.13 ug/L 0.00 Spiked Amount 5.000 Recovery = 102.60%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 11618 0.21 ug/L # 15 20) Dimethylphthalate 18.34 163 467822 2.43 ug/L # 55 21) 2,6-Dinitrotoluene 18.34 165 371847 9.91 ug/L # 17 35) Di-n-butylphthalate 24.85 149 9108 0.03 ug/L 95 41) Benzo(a)anthracene 30.50 228 9090 0.04 ug/L # 48 42) Bis(2-ethylhexyl )phthalate 31.10 149 8450 0.59 ug/L 91 43) Chrysene 30.50 228 9090 0.04 ug/L + 46 48) Benzo(a)pyrene 34.42 252 10276 0.05 ug/L h 1

(#) = qualifier out of range (m) = manual integration 00739.D SCAN508.M Thu Jan 17 08:12:26 2002 Page 1

NYC-WTC_000051969

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NYC-WTC_000051969Source: NYC Law Department, mirrored locally

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