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GCMS results for sample AE00704, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00704 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051914–000051929

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051920
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN16\00704.D Vial: 4 • Acq On : 16 Jan 2002 5:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ****************************************************** * * * * ** * * * * * * * k *

Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 3.48 0.12 ug/L 42154 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 59 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 50 4 Acetonitrile, dichloro- ____________ 109 C2HC12N 003018-12-0 37 Abundance Scan 9 (3.476 min): 00704.D (-) m/z 74.00 100.00% 74

82 5000 47

39 3.50 3.60 3.70 3.80 3.90 Il........................... I m/ z 82.00 55.24% 0! ............................. I',' ।................. m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 82 44 TT I ' 1 ' ■ i 3.50 3.60 3.70 3.80 3.90 TTT 47 m/z 76.00 36.58% 35 0 ,' .I ................. Ij |I ' 1 ’ 1 1 1 ' ' ' I ' ' 1 ' I ' ' ' 1 I rtt ■ i ■ ■ • • i > I ! 109 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 3.50 3.60 3.70 3.80 3.90 5000 m/ z 84.00 33.46% 47

12 35 108 0! 2.. P.. i -J. । _________ L ' I ' ' 1 1 I ' ■n-* • i 1 > 1 1 ITT * । roT m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 3.50 3.60 3.70 3.80 3.90 m/z 47.00 31.66% 47 82 5000

38

m/z-> 0 ■ 1 i ■ ■ ■ ■ । 1 ■ ' ■ i ■ ■ 10 20 30 | i ■ ' 40 50 i ■ ' ' ■ i ' ' ■ ' i ■ 60 70 I 80 95 102108 +,——TT 90 100 110 A 3.50 3.60 3.70 3.80 3.90

10704.D SCAN508.M Thu Jan 17 08:17:34 2002 Page 3

NYC-WTC_000051920

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NYC-WTC_000051920Source: NYC Law Department, mirrored locally

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