GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051877–000051894Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN16\00701.D Vial: 1 . Acq On : 16 Jan 2002 3:07 pm Operator: Sample : 508scan Inst : Ins t rumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
5.89 4.03 ug/L 1244780 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00701 .D (-) m/z 73.10 100.00% 73
5000
m/z-> 43
87 103 0 111 r rr 1 0,1555... , Vp—P*1*9*mWWTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 TT m/z 5.60 5.80 43.10 L 6.00 6.20 23.39% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.41% 27 55 87 113 174 0 poodaunne i'11' ■ i " ■ ■ i ■ ■ ■ ■ i1 Pm MT
L i '-1 ■ ■ i ■ ■ ■ ■ i " • ■ r ■ " i' " ' i r 1' ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ‘ I‘* 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.05% 43 27 55 .1 87 113 174 0-TPTT4 TIUnmm +pr r‘ । i-i < > 11 ■ ■ ■ i > । > ■ ।1 > |-,-ni 111111111 •111 ■ rn/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... ‘ I’ 73 5.60 m/z 5000 55 87
n/z-> 27 45 | 0-T 11 ■ i' ' I' ''' 11 m । ■ i' " 11'' ■ • r ''' i'1 " i ■ " ' r ''' i ■ ■ " i ■ " ' i''' ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 TT ■ ' ’ I ' ‘ 5.60 ' I ' ' ' ' I ' ' ' ' I ' ' 5.80 6.00 6.20
30701.D SCAN508.M Thu Jan 17 08:17:15 2002 Page 5
NYC-WTC_000051885
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NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder