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GCMS results for sample AE00700, Feb 13 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.

NYC-WTC_000051806–000051824

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\5973N\02FEB01\00700.D Vial: 7 - Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.477 7 9 17 rVB 34974 60555 0.44% 0.086% 2 3.602 17 20 25 rBV 33984 58091 0.43% 0.083% 3 3.762 29 34 45 rW2 7686 24622 0.18% 0.035% 4 3.910 45 47 53 rW 18738 31060 0.23% 0.044% 5 5.931 221 224 227 rBV 59830 133137 0.97% 0.190%

6 6.000 227 230 243 rVB 31205 82820 0.61% 0.118% 7 9.710 551 555 561 rBV 3807336 7654659 56.02% 10.910% 8 9.859 565 568 579 rVB 18658 60656 0.44% 0.086% 9 12.542 799 803 807 rW 17921 29425 0.22% 0.042% 10 13.192 855 860 865 rBV 5879420 11115561 81.35% 15.843%

11 13.375 873 876 881 rVB 11106 19514 0.14% 0.028% 12 16.549 1151 1154 1159 rBV 17346 32345 0.24% 0.046% 13 18.341 1305 1311 1315 rBV 6248205 12418142 90.88% 17.699% 14 22.280 1653 1656 1661 rVB2 45690 89349 0.65% 0.127% 15 22.634 1681 1687 1693 rBV2 5914532 13663910 100.00% 19.475%

16 22.771 1697 1699 1717 rVB2 80159 286994 2.10% 0.409% 17 27.726 2129 2133 2139 rBV 899260 1569822 11.49% 2.237% 18 30.489 2369 2375 2401 rBV2 4924923 12746144 93.28% 18.167% 19 31.105 2423 2429 2441 rVB5 13294 54123 0.40% 0.077% 20 34.416 2713 2719 2759 rBV 3629182 10031232 73.41% 14.297%

Sum of corrected areas: 70162161

0700.D SCAN508.M Mon Feb 04 08:40:50 2002 Page 1

NYC-WTC_000051810

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NYC-WTC_000051810Source: NYC Law Department, mirrored locally

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