GCMS results for sample AE00557, Jan 17 2002

NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02JAN15\00557 . D Vial: 1 Acq On : 15 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Aniline Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.05 0.17 ug/L 53131 1,4 -Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm C Qual

1 Aniline 93 C6H7N 000062-53-3 90 2 Aniline $$ Benzenamine $$ Aminob... 93 C6H7N 000062-53-3 90 3 Aniline 93 C6H7N 000062-53-3 90 4 Benzenamine (CAS) $$ Aniline $$ ... 93 C6H7N 000062-53-3 90 Abundance Scan 497 (9.048 min): 00557.D (-) m/ z 93.10 100.00% 93

5000 66 .. TTT 39 46 50 8.60 8.80 9.00 9.20 9.40 Ol .. ... ---HH* ■ I ■111 I -' I > r 11111111111111'11 "maur m/z 66.10 32.56% m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5666: Aniline 93

5000 8.60 8.80 9.00 9.20 9.40 66 m/z 65.10 14.11% 37 46 52 62 78 0+ 1 11 ' 1' ' I ' 1 1 1 11 1 1 1 I 1 1 1 ' I 1 1 ' 1 i ■ ' ' ■ i ' 1 1 11 1 ■' i' ■ ' ■ i ■ ■1 ■ i ■ ■ ■' i ■ ■ ■ ■ i ■ I mr ■ i ’" m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5668: Aniline $$ Benzenamine $$ Aminobenzene $$ Aminophen... 93

8.60 8.80 9.00 9.20 9.40 5000 m/z 39.10 9.60% 66

54 77 0+ ' 11 > ■ > 11 1 ■ ’ ■ i' ■ • > i ■ ■' ■ । 11111' ■ ... l ■ ■ । ■ ■ ■ ■ । ■ 11 • । • i ■ —P n/z-> 30 35 40 45 50 55 60 65 70 75 80 85 95 100 Abundance #5667: Aniline 93 8.60 8.80 9.00 9.20 9.40 m/z 92.00 9.46% 5000 66

37 ............................ .. 0 TPPP , 76............... 1 " I " " 11 " 1111 "C —PP mtz-> 30 35 40 45 50 55 60 65 70 75 80 85 95 100 8.60 8.80 9.00 9.20 9.40

00557.D SCAN508.M Wed Jan 16 08:13:57 2002 Page 5

NYC-WTC_000051776