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GCMS blank analysis for sample AE00555, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051515
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal .- TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 33532 51376 0.35% 0.066% 2 3.910 45 47 51 rVB 12416 21080 0.14% 0.027% 3 4.253 73 77 85 rVB4 9470 28388 0.19% 0.036% 4 4.630 107 110 119 rVB2 15943 36317 0.25% 0.046% 5 4.847 125 129 139 rBV4 19530 76299 0.52% 0.097%

6 5.006 139 143 149 rVB3 11546 27816 0.19% 0.035% 7 5.885 215 220 243 rVB 796312 1645943 11.25% 2.100% 8 9.710 551 555 561 rBV 4430639 8739383 59.75% 11.151% 9 12.542 799 803 807 rVB2 48663 81429 0.56% 0.104% 10 13.192 855 860 865 rBV 6602695 12499879 85.47% 15.949%

11 16.549 1149 1154 1159 rVB 12458 22910 0.16% 0.029% 12 18.341 1305 1311 1315 rBV 6985472 13567485 92.77% 17.312% 13 22.280 1653 1656 1661 rBV2 47019 89849 0.61% 0.115% 14 22.645 1681 1688 1693 rBV 6440076 14625494 100.00% 18.662% 15 22.771 1697 1699 1717 rVB 75416 209940 1.44% 0.268%

16 24.849 1875 1881 1885 rW 17308 35251 0.24% 0.045% 17 27.726 2127 2133 2139 rVB 865786 1566927 10.71% 1.999% 18 29.678 2299 2304 2311 rW 7082 24567 0.17% 0.031% 19 30.500 2369 2376 2381 rBV 5500927 13557484 92.70% 17.299% 20 34.416 2713 2719 2747 rBV 4286358 11463824 78.38% 14.628%

Sum of corrected areas: 78371641

109B.D SCAN508.M Wed Jan 30 09:02:32 2002 Page 1

NYC-WTC_000051515

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NYC-WTC_000051515Source: NYC Law Department, mirrored locally

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