GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 17 21 25 rBV 53015 82186 0.37% 0.069% 2 4.241 73 76 79 rBV 150685 261555 1.16% 0.220% 3 5.920 219 223 235 rBV 78898 180036 0.80% 0.152% 4 9.082 493 500 509 rW3 24042 87972 0.39% 0.074% 5 9.242 509 514 521 rW3 25989 76315 0.34% 0.064%

6 9.710 551 555 561 rBV 7070335 13131619 58.48% 11.065% 7 13.192 855 860 865 rBV 9292784 18900981 84.18% 15.926% 8 17.885 1265 1271 1277 rVB2 24386 82225 0.37% 0.069% 9 18.341 1305 1311 1315 rBV 9582069 20582527 91.66% 17.343% 10 18.421 1315 1318 1329 rVB 64180 179260 0.80% 0.151%

11 19.997 1451 1456 1463 rVB3 40412 123473 0.55% 0.104% 12 20.465 1489 1497 1501 rBV2 22109 71635 0.32% 0.060% 13 22.280 1651 1656 1661 rBV2 105614 189929 0.85% 0.160% 14 22.645 1681 1688 1693 rBV2 9152567 22454317 100.00% 18.920% 15 22.771 1697 1699 1719 rVB2 126933 447998 2.00% 0.377%

16 26.847 2051 2056 2061 rBV 31790 74418 0.33% 0.063% 17 27.726 2127 2133 2139 rBV 1361005 2444042 10.88% 2.059% 18 30.500 2369 2376 2381 rBV2 7714048 21294947 94.84% 17.943% 19 31.105 2425 2429 2437 rVB2 28238 78278 0.35% 0.066% 20 34.428 2713 2720 2751 rBV 6106776 17937449 79.88% 15.114%

Sum of corrected areas: 118681162

0201B.D SCAN508.M Thu Feb 21 10:18:56 2002 Page 1

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