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GCMS blank analysis for sample AE00314, Jan 15 2002

Machine-extracted title · confidence 100%

Laboratory report documenting a method blank analysis to verify absence of contamination during gas chromatography-mass spectrometry testing.

NYC-WTC_000051353–000051363

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051356
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\l\5973N\02JAN14\0108BA.D Vial: 1 Acq On : 14 Jan 2002 10:28 am Operator: Sample : lab blank 1/8 a Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 4.835 125 128 139 rBV3 24889 69729 0.73% 0.129% 2 5.885 217 220 243 rW 580414 1263266 13.24% 2.331% 3 8.854 477 480 485 rVB 36744 67494 0.71% 0.125% 4 9.710 551 555 561 rBV 2838006 5764676 60.42% 10.638% 5 13.192 855 860 865 rBV 4356604 8210759 86.06% 15.152%

6 18.341 1305 1311 1315 rBV 4548900 8955464 93.86% 16.527% 7 22.280 1653 1656 1661 rW 31524 61196 0.64% 0.113% 8 22.634 1681 1687 1693 rBV2 4337566 9540810 100.00% 17.607% 9 22.771 1695 1699 1711 rW 45618 128906 1.35% 0.238% 10 27.726 2129 2133 2139 rBV 759456 1303571 13.66% 2.406%

11 30.489 2369 2375 2381 rBV2 4128145 9431783 98.86% 17.406% 12 31.105 2421 2429 2449 rVB4 29622 119679 1.25% 0.221% 13 32.818 2575 2579 2595 rBV 28425 94475 0.99% 0.174% 14 33.446 2629 2634 2635 rBV 37180 91566 0.96% 0.169% 15 33.503 2635 2639 2657 rVB 67805 293648 3.08% 0.542%

16 34.245 2699 2704 2713 rBV5 9367 40872 0.43% 0.075% 17 34.416 2713 2719 2741 rW 3221574 8134918 85.26% 15.012% 18 37.008 2941 2946 2949 rBV2 25928 84082 0.88% 0.155% 19 37.099 2949 2954 2971 rVB 47614 281023 2.95% 0.519% 20 37.704 3001 3007 3027 rBV 39697 250200 2.62% 0.462%

Sum of corrected areas: 54188117

0108BA.D SCAN508.M Tue Jan 15 08:47:57 2002 Page 1

NYC-WTC_000051356

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