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GCMS analysis results for sample AE00466, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 5.885 217 220 251 rVB 829124 1664760 12.57% 2.310% 2 9.710 551 555 561 rW 3375205 6512106 49.18% 9.036% 3 13.192 855 860 865 rBV 4925352 9242804 69.80% 12.825% 4 18.341 1305 1311 1315 rBV 5172297 10391877 78.48% 14.419% 5 20.613 1501 1510 1515 rBV 108638 365905 2.76% 0.508%

6 21.412 1575 1580 1585 rW 449051 1100903 8.31% 1.528% 7 22.052 1631 1636 1639 rVB3 69391 196935 1.49% 0.273% 8 22.645 1681 1688 1693 rBV2 5205577 11833958 89.37% 16.420% 9 22.794 1695 1701 1705 rW2 620448 1442483 10.89% 2.002% 10 23.559 1765 1768 1769 rBV3 101154 238230 1.80% 0.331%

11 23.856 1789 1794 1799 rBV3 255998 823301 6.22% 1.142% 12 23.947 1799 1802 1807 rBV2 131728 295688 2.23% 0.410% 13 24.118 1813 1817 1821 rBV3 108799 210935 1.59% 0.293% 14 26.059 1983 1987 1995 rVB2 246611 840383 6.35% 1.166% 15 27.737 2129 2134 2137 rBV 732363 1363086 10.29% 1.891%

16 27.840 2139 2143 2147 rBV 266546 894033 6.75% 1.241% 17 30.500 2371 2376 2381 rBV2 4858050 13241710 100.00% 18.374% 18 34.428 2713 2720 2725 rVB 3982822 10454445 78.95% 14.506% 19 35.798 2837 2840 2845 rVB2 105198 225447 1.70% 0.313% 20 36.563 2903 2907 2923 rVB3 178241 729478 5.51% 1.012%

Sum of corrected areas: 72068467

0473.D SCAN508.M Fri Jan 11 10:09:08 2002 Page 1

NYC-WTC_000051267

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NYC-WTC_000051267Source: NYC Law Department, mirrored locally

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