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GCMS analysis results for sample AE00473, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.

NYC-WTC_000051252–000051262

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00366.D Vial: 2 Acq On 10 Jan 2002 3:39 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 19 21 25 rVB 25485 45748 0.40% 0.069% 2 4.835 125 128 141 rW4 25187 73657 0.65% 0.111% 3 5.885 217 220 239 rBV 721388 1399076 12.26% 2.117% 4 9.710 551 555 561 rW 3291020 6441008 56.44% 9.748% 5 13.192 855 860 865 rBV 4810647 9066322 79.44% 13.722%

6 18.341 1305 1311 1315 rBV 5019203 9903168 86.78% 14.988% 7 22.280 1651 1656 1661 rBV2 39890 71694 0.63% 0.109% 8 22.645 1681 1688 1693 rBV 4866268 10906909 95.57% 16.507% 9 22.771 1695 1699 1723 rW 56999 213743 1.87% 0.323% 10 27.726 2129 2133 2139 rVB 882395 1570761 13.76% 2.377%

11 30.489 2369 2375 2381 rBV 4570970 11412211 100.00% 17.272% 12 31.105 2425 2429 2451 rVB 190995 637279 5.58% 0.965% 13 32.829 2575 2580 2613 rBV 117821 571617 5.01% 0.865% 14 33.446 2629 2634 2635 rBV 117334 266918 2.34% 0.404% 15 33.503 2635 2639 2655 rVB 180066 622271 5.45% 0.942%

16 34.245 2699 2704 2713 rBV2 74530 263488 2.31% 0.399% 17 34.416 2713 2719 2745 rVB 3969026 10161710 89.04% 15.380% 18 37.019 2941 2947 2951 rBV 135137 520205 4.56% 0.787% 19 37.099 2951 2954 2973 rVB 214717 1002487 8.78% 1.517% 20 37.716 3001 3008 3025 rBV 212044 922536 8 : 08% 1.396%

Sum of corrected areas: 66072808

00366.D SCAN508.M Fri Jan 11 10:08:24 2002 Page 1

NYC-WTC_000051256

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