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GCMS analysis results for sample AE00366, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.

NYC-WTC_000051236–000051251

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00465.D Vial: 3 Acq On 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 15 20 25 rBV 35472 59196 0.53% 0.096% 2 4.618 107 109 117 rVB2 15096 32725 0.29% 0.053% 3 4.846 123 129 141 rBV3 17846 61208 0.55% 0.099% 4 5.006 141 143 151 rVB 28842 52099 0.47% 0.084% 5 5.885 217 220 243 rBV 788067 1646849 14.74% 2.668% 6 9.539 539 540 54 5 rW 20840 49021 0.44% 0.079% 7 9.630 545 548 551 rW 27262 57892 0.52% 0.094% 8 9.710 551 555 561 rW 3198876 6328579 56.66% 10.253% 9 9.836 561 566 581 rVB 27781 102790 0.92% 0.167% 10 12.541 799 803 809 rVB 19608 31040 0.28% 0.050% 11 13.192 855 860 865 rBV 4887647 9122290 81.67% 14.779% 12 18.341 1305 1311 1315 rBV 5101840 10176468 91.11% 16.487% 13 22.280 1653 1656 1659 rW 39812 70443 0.63% 0.114% 14 22.634 1681 1687 1693 rBV2 4955470 11080643 99.21% 17.952% 15 22.771 1695 1699 1713 rVB 60601 176627 1.58% 0.286% 16 27.726 2129 2133 2139 rW 1020453 1789899 16.03% 2.900% 17 29.678 2299 2304 2311 rVB3 9070 23851 0.21% 0.039% 18 30.489 2369 2375 2381 rBV 4600337 11169052 100.00% 18.095% 19 31.105 2421 2429 2441 rVB4 16545 76053 0.68% 0.123% 20 34.416 2713 2719 2753 rBV 3831296 9617303 86.11% 15.581%

Sum of corrected areas: 61724028

)0465.D SCAN508.M Fri Jan 11 10:08:28 2002 Page 1

NYC-WTC_000051240

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NYC-WTC_000051240Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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