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← Document results/DEP Box 28/GCMS X 1/8/02 A 1/10/02
Document / 16 pages

GCMS analysis results for sample AE00328, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00328 conducted on January 18, 2002.

NYC-WTC_000051206–000051221

Folder label: “GCMS X 1/8/02 A 1/10/02”

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Scanned page image, NYC-WTC_000051214
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00327.D Vial: 3 Acq On 10 Jan 2002 2:00 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 2-Butenal, 3-methyl- (CAS) ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

4.86 0.15 ug/L 48568 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H80 000107-86-8 58 2 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H8O 000107-86-8 58 3 Furan, 2,3-dihydro-4-methyl- 84 C5H80 034314-83-5 53 4 2-Pentenal, (E)- $$ trans-2-Pent... 84 C5H8O 001576-87-0 53 Abundance Scan 130 (4.858 min): 00327.D (-) m/ z 83.95 100.00%

W 55 84

41 5000 59 MV/WA) 51

4.60 4.80 5.00 5.20 01 ■ ■ i ■' ■ ■ i''' ■ i ■ ■ ■ ■ i ■ ■ ' ■ r 1 । ■. • • । ■ '11 " " I " PT '111'11 m/z 55.10 90.90% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3221: 2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal $$... 8)4 55

39 5000 27 4.60 4.80 5.00 5.20 m/z 83.10 „L 63.84% 44 69 Of । "TTT r ‘ r ' 111 1 I •1 '' I' 11111111111111'' i11 ■ ■ i' ■ ■ ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3222: 2-Butenal, 3-methyl- $$ Crotonaldehyde, 3-methyl- $... 84 55 TBdrn/m. 4.60 4.80 5.00 5.20 5000 39 m/z 41.10 54.55% 27

o ' ■ i ■'' ■ i 1 '1111'11 ■ । ■ ‘ 111111' 44 L — n......... 69 I ' ■' ■ i1 1 ' ' i m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 #3350: Furan, 2,3-dihydro-4-methyl- 80 85 90 A NWA A \ A r',1 Ifp-yPTu i 1 i ‘| il 1'|> T | 1 1 1 1 55 84 4.60 4.80 5 00 5.20 m/z 39.10 53.22%

5000 41 27

m/z-> 37 0 ■ ■ । 1' 1 ‘ I । .... 1" 20 25 30 35 40 45 50 55 44 —P 51 69 ■ i'' ■' i' ■'11 ■ ■ ’11 ■ ■ ■' i'r

60 65 70 75 80 85 1 i ■1 111 90 JOI 4.60 4.80 5.00 ' ' i ' ■' 5.20

'0327.D SCAN508.M Fri Jan 11- 10:08:16 2002 Page 5

NYC-WTC_000051214

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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