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GCMS analysis results for sample AE00307, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051055–000051072

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

yuantitatlon Keporc (NOC Reviewed)

Data File : C : \MSDCHEM\1\5973N\02JAN08\307 . D Vial: 6 Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 09 12:51:24 2002 Quant Results File: SCANS08.RES

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Last Update : Wed Jan 09 12:49:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1166237 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4837376 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2445795 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 4043393 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3794970 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2681370 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 324371 5.08 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.60%

Target Compounds Qvalue 2) N-nitroso-dimethylamine 3.60 74 11676 0.23 ug/L # 12 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. \ 7) 2,2'-oxybis (1-Chloropropa 0.00 45 0 N.D. \ 8) N-nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy) metha 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.Di 19) 2-Chloronaphthalene 0.00 162 0 N.D.\ 20) Dimethylphthalate 18.34 163 394099 2.44 /L # 55 21) 2,6-Dinitrotoluene 18.34 165 314805 9.99 u /L # 17 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. \ 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzene 0.00 77 0 N.D. 30) N-nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D.

(#) = qualifier out of range (m) = manual integration 307.D SCAN508.M Wed Jan 09 12:51:25 2002 Page 1

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