GCMS reference data for sample AE00275, Jan 2002

NYC 9/11 Public Portal Document

yuancitaclon Keporc (NOU Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN08\0107REF.D Vial: 2 Acq On : 8 Jan 2002 6:16 pm Operator: Sample : ref ext 1/7/02 Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 09 12:51:18 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Wed Jan 09 12:49:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1181722 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5092582 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2697766 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.65 188 4509737 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 3999538 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2952916 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 382603 5.37 ug/L 0.00 Spiked Amount 5.000 Recovery = 107.40%

Target Compounds Qvalue 2) N-nitroso-dimethylamine 3.99 74 155681 3.09 ug/L 52 3) bis (2-Chloroethyl) ether 9.24 93 366757 4.52 ug/L 72 4) 1,3-Dichlorobenzene 9.61 146 184041 2.08 ug/L 95 5) 1,4-Dichlorobenzene 9.76 146 198493 2.23 ug/L 96 6) 1,2-Dichlorobenzene 10.24 146 210953 2.67 ug/L 100 7) 2,2'-oxybis (1-Chloropropa 10.67 45 522815 3.83 ug/L # 73 8) N-nitroso-di-n-propylamine 11.05 70 248993 3.99 ug/L 77 9) Hexachloroethane 11.03 117 34928 1.10 ug/L 96 11) Nitrobenzene 11.35 77 289158 3.04 ug/L 82 12) Isophorone 12.03 82 700622 4.08 ug/L 91 13) bis (2-Chloroethoxy) metha 12.77 93 467582 4.59 ug/L 90 14) 1,2,4-Trichlorobenzene 13.11 180 171361 2.58 ug/L 97 15) Naphthalene 13.25 128 941535 3.86 ug/L 98 16) Hexachlorobutadiene 13.84 225 33415 0.95 ug/L 99 18) Hexachlorocyclopentadiene 15.96 237 7276 0.30 ug/L 98 19) 2-Chloronaphthalene 16.65 162 536804 3.60 ug/L 91 20) Dimethylphthalate 17.88 163 770732 4.33 ug/L 93 21) 2,6-Dinitrotoluene 18.06 165 97597 2.81 ug/L 79 22) Acenaphthylene 17.86 152 899894 4.14 ug/L 97 23) Acenaphthene 18.42 153 646270 4.18 ug/L 97 24) 2,4-Dinitrotoluene 19.17 165 118296 2.60 ug/L 92 25) Diethylphthalate 20.00 149 793120 4.65 ug/L 97 26) 4-Chlorophenyl-phenylether 20.02 204 333980 4.65 ug/L 86 27) Fluorene 19.91 166 776596 4.41 ug/L 97 28) Azobenzene 20.46 77 859592 4.04 ug/L 85 30) N-nitrosodiphenylamine 20.43 169 484594 4.24 ug/L 98 31) 4-Bromophenyl-phenylether 21.44 248 195683 4.17 ug/L 89 32) Hexachlorobenzene 21.77 284 191414 3.86 ug/L 95 33) Phenanthrene 22.70 178 1216886 4.90 ug/L 99 34) Anthracene 22.83 178 1059302 4.39 ug/L 99

(#) = qualifier out of range (m) = manual integration 0107REF.D SCAN508.M Wed Jan 09 12:51:19 2002 Page 1

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