GCMS analysis results for sample AE00308, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051073–000051087

Folder label: “GCMS X 1/7/02 A 1/8/02”

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NYC 9/11 Public Portal Document

yuantitatlon Keporc (NOC Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN08\308.D Vial: 7 Acq On : 8 Jan 2002 10:28 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiple: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 09 12:51:25 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Wed Jan 09 12:49:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1161749 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 4872148 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2492466 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 4045126 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3506485 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2445437 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 299594 4.69 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.80%

Target Compounds 2) N-nitroso-dimethylamine 3) bis (2-Chloroethyl) ether 4) 1,3-Dichlorobenzene 5) 1,4-Dichlorobenzene 6) 1,2-Dichlorobenzene 7) 2,2'-oxybis (1-Chloropropa 8) N-nitroso-di-n-propylamine 9) Hexachloroethane 11) Nitrobenzene 12) Isophorone 13) bis (2-Chloroethoxy) metha 14) 1,2,4-Trichlorobenzene 15) Naphthalene 16) Hexachlorobutadiene 18) Hexachlorocyclopentadiene 19) 2-Chloronaphthalene 20) Dimethylphthalate 21) 2,6-Dinitrotoluene 22) Acenaphthylene 23) Acenaphthene 24) 2,4-Dinitrotoluene 25) Diethylphthalate 26) 4-Chlorophenyl-phenylether 27) Fluorene 28) Azobenzene 30) N-nitrosodiphenylamine 31) 4-Bromophenyl-phenylether 32) Hexachlorobenzene 33) Phenanthrene 34) Anthracene Qvalue 3.59 74 7155 0.14 /L # 24 0.00 93 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 45 0 N.D. 0.00 70 0 N.D. 0.00 117 0 N.D. 0.00 77 0 N.D. 0.00 82 0 N.D. 0.00 93 0 N.D. 0.00 180 0 N.D. 0.00 128 0 N.D. 0.00 225 0 N.D. 0.00 237 0 N.D N.D. 0.00 162 0 18.34 163 406250 2.47 u L # 56 18.34 165 322853 10.06 ug L # 17 0.00 152 0 N.D. 0.00 153 0 N.D. 0.00 165 0 N.D. 0.00 149 0 N.D. 0.00 204 0 N.D. 0.00 166 0 N.D. 0.00 77 0 N.D. 0.00 169 0 N.D. 0.00 248 0 N.D. 0.00 284 0 N.D. 0.00 178 0 N.D. 0.00 178 0 N.D.

(#) = qualifier out of range (m) = manual integration 308.D SCAN508.M Wed Jan 09 12:51:26 2002 Page 1

NYC-WTC_000051074

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GCMS analysis results for sample AE00309, Jan 2002 · Box DEP Box 28

NYC-WTC_000051088

Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.

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