GCMS surrogate recovery results for sample AE00280, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2JAN09\280.D Vial: 5 Acq On 9 Jan 2002 9:31 pm Operator: ■ Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.11 ug/L 54381 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 25 Abundance Scan 9 (3.476 min): 280.D (-) m/z 74.00 100.00% 714

82 5000 47 ............ 38 350 3.60 3.70 3.80 3.90 01 ............................ ' I ' ' 1 ■ I ' ' ■ 1 I| 1 1II. 1 , 1 . 1 , 1|l,Il, ' , , ' I 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ' i ■ m/z 81.90 59.50% * I ' ' ' ' I ' n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 Al i ■ • • ■ i' ■ ■ ■ i ■ ' ■ ■ i

47 3.50 3.60 3.70 3.80 3.90 m/z 76.00 35.67% 35

m/z-> 0+ ■ I ‘ 10 ' I ' 20 30 _L __________ L 1 .......... . 1 1 1 1 1 1 1 ' 1 • i • ' ' • i ' 40 50 60 70 80 90 ।.... 109— 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- 7l4 82 3.50 3.60 3.70 3.80 3.90 5000 m/z 83.90 25.91% 47 35 12 Of -PPPP —+ ll............' 1......... 194.. rn/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- I ' ' ' ' I I’’ ‘* I 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 23.32%

5000 82 47

m/z-> 0 ■ i

10 ' ■

20 i ■ ■ ' ‘

30 i ■ — ' ' I ' ' ' ' I ' 40 50 60 70 80 1 1 I 1 1 1 1 I 1 1 1 1 I 1 90 100 110 A T 3.50 3.60 3.70 3.80 3.90

280.D SCAN508.M Thu Jan 10 11:51:54 2002 Page 3

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