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GCMS analysis results for sample AE00165, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.

NYC-WTC_000050664–000050682

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB04\00165 . D Vial: 4 • Acq On : 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 TRIPROPYLENE GLYCOL 2 Concentration Rank 7 R.T. EstCono Area Relative to ISTD R.T. 9.63 0.14 ug/L 67868 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 72 1— 2 TRIPROPYLENE GLYCOL 1 192 C9H20O4 000000-00-0 72 62 3 2-Propanol, 1,1’-oxybis- (CAS) $... 134 C6H1403 000110-98-5 59 MetC 4 4-(Dimethylamino) -1,3-diazaspiro... 209 C11H19N3O 000000-00-0 59 Abundance Scan 548 (9.630 min): 00165. D (-) m/z 59.10 100.00% 59

5000 45 103 73 9.20 9.40 9.60 9.80 10.00 O.. | I'.1. jsa dI .. 1 , | A | I .... | JI 1 | | I I I I | I I I | | I l 1 I | | !> | | I 1 !! | | I I | ) m/z 45.10 41.48% nfe-> 20 30 40 50 60 70 80 M 100 110 120 130 140 150 160 Abundance #102327: TRIPROPYLENE GLYCOL 2

5000 —----- 9.20 9.40 9.60 9.80 10.00 45 103 m/z 103.10 33.44%

n/z—> 0 117, 9, 117 130 161 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 • । ‘ । ■11 ■ i ■ ■' • i • ■ ■ ■ । • ■ ■ ■ । ■ ■ ■ * ।

Abundance #102326: TRIPROPYLENE GLYCOL 1 59 _ ..... 9.20 9.40 9.60 9.80 10.00 5000 Wz 73.10 21.87% 45 103 72 |, 117 130 0f| r । 1 1 | । । 11 | I TInr 1 " I ' ' ‘ 1 1

. M.., ' I " ' 1 I ' 1 1 1 I ' 1 ■ ■ | | । ri-i | < i i >1 i i i i । i i > i । i i i i |' iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance ;#29204:2-Propanol, 1,1’-oxybis- (CAS) $$ Dipropylene glyc... 59 9.20 9.40 9.60 9.80 10.00 m/z 41.10 19.63% 5000 31 A 45 103

0- i1 ‘ ■ i ■ ■ “ i t-ttt —4 B****h****I*d*IGBBaamaam 17T1 11 > । < 11 > 111111111111 n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 9.40 9.60 9.80 10.00

>0165.D SCAN508.M Tue Feb 05 09:47:34 2002 Page 9

NYC-WTC_000050676

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NYC-WTC_000050676Source: NYC Law Department, mirrored locally

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